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The results of a study of the effect of microvolume emission (power 700 W, frequency 2.45 GHz) on the structural changes in natural clay particles are presented. The influence of the irradiation time (10 and 20 minutes) and the environment…

Materials Science · Physics 2023-02-14 Anna G. Chetverikova , Marina M. Filyak , Olga N. Kanygina

We present experimental results on crystal--amorphous transition of forsterite (Mg2SiO4) silicate under ion irradiation. The aim of this work is to study the structural evolution of one of the most abundant crystalline silicates observed in…

Astrophysics · Physics 2009-11-10 J. R. Brucato , G. Strazzulla , G. Baratta , L. Colangeli

Microwave energy has been demonstrated to be beneficial for reducing the energetic cost of several steps of the mining process. Significant literature has been developed about this topic but few studies are focused on understanding the…

Materials Science · Physics 2015-10-30 Tamara Monti , Alexander Tselev , Ofonime Udoudo , Ilia N. Ivanov , Samuel W. Kingman

Water vitrifies if cooled at rates above $3 \cdot 10^5$ K/s. Surprisingly, this process cannot simply be reversed by heating the resulting amorphous ice at a similar rate. Instead, we have recently shown that the sample transiently…

Chemical Physics · Physics 2024-02-01 Constantin R. Krüger , Nathan J. Mowry , Marcel Drabbels , Ulrich J. Lorenz

Microwave heating of methane hydrate is investigated with electrostatic molecular dynamics simulations by the SPC/E water model. The structure I of methane hydrate is constructed. When the methane hydrate with a density of 0.91…

Chemical Physics · Physics 2023-11-27 Motohiko Tanaka , Motoyasu Sato , Shin Nakatani

Microwave-assisted hydrothermal synthesis was used to grow LiMnPO$_4$ micro- and nanocrystals from acetate precursors. By appropriate adjustment of the precursor concentration and the pH-value of the reactant, the product composition and…

Materials Science · Physics 2014-05-29 Christoph Neef , Carsten Jähne , Hans-Peter Meyer , Rüdiger Klingeler

In order to study the heating process of water by the microwaves of 2.5-20GHz frequencies, we have performed molecular dynamics simulations by adopting a non-polarized water model that have fixed point charges on rigid-body molecules. All…

Materials Science · Physics 2009-11-11 Motohiko Tanaka , Motoyasu Sato

Water-free NH4V3O8 microcrystals have been successfully synthesized by a microwave-assisted hydrothermal method. The products were characterized by means of X-ray diffraction, scanning electron microscopy, Fourier transform infrared…

Materials Science · Physics 2016-09-21 G. S. Zakharova , A. Ottmann , B. Ehrstein , R. Klingeler

Photocatalytic- and Photoelectrochemical water splitting is currently performed using radiation sources with wavelengths < 1000 nm, i.e. in the near infrared range (NIR). The fact that water has a broad absorption band, which lies at…

Chemical Physics · Physics 2023-01-16 Klara Ruewe , Helmut Schaefer

Spherical quartz stones of around 1 cm in diameter have been exposed to anodic arc discharges in a helium atmosphere at 300 Torr. The arc current flowing between the graphite electrodes was set either in continuous DC mode (30-150 A) or in…

Plasma Physics · Physics 2021-03-04 Carles Corbella , Sabine Portal , Michael Keidar

Crystalline to amorphous phase transformation during initial lithiation in (100) silicon-wafers is studied in an electrochemical cell with lithium metal as the counter and reference electrode. It is demonstrated that severe stress jumps…

The crystal structure of CH3NH3PbBr3 perovskite has been investigated under high-pressure by synchrotron-based powder X-ray diffraction. We found that after the previously reported phase transitions in CH3NH3PbBr3 (Pm-3m->Im-3->Pmn21),…

The use of microwave irradiation is a promising alternative heat source for the synthesis of inorganic materials such as perovskite oxides. The method offers massive energy and time savings as compared to the traditional ceramic method. In…

Materials Science · Physics 2014-01-10 Jesus Prado-Gonjal , Rainer Schmidt , Emilio Moran

We study a model of interacting particles in two dimensions to address the relation between crystal-crystal transformations and pressure-induced amorphization. On increasing pressure at very low temperature, our model undergoes a…

Materials Science · Physics 2009-11-11 S. Bustingorry , E. A. Jagla

The microwave sintering homogeneity of large and complex shape specimens is analyzed. A new approach enabling the fabrication of complex shapes ceramics via 3D printing and microwave sintering is presented. The use of a dental microwave…

Materials Science · Physics 2020-11-26 Charles Manière , Shirley Chan , Eugene A. Olevsky

Two sets of amorphous carbon materials prepared at different routes are irradiated with swift (145 MeV) heavy ion (Ne6+). The structural parameters like the size of ordered grains along c and a axis i.e. Lc & La, the average spacing of the…

Materials Science · Physics 2007-05-23 A. Sarkar , K. Dasgupta , P. Barat , P. Mukherjee , D. Sathiyamoorthy

The valence of iron has been used in terrestrial studies to trace the hydrolysis of primary silicate rocks. Here, we use a similar approach to characterize the secondary processes, namely thermal metamorphism and aqueous alteration, that…

Earth and Planetary Astrophysics · Physics 2021-04-02 A. Garenne , P. Beck , G. Montes-Hernandez , L. Bonal , E. Quirico , O. Proux , J. L. Hazemann

The amorphous phases of antimony oxide at three different oxidation levels have been investigated by {\it ab initio} molecular-dynamics calculations using a simulated `melt-quench' approach. The atomic and electronic structure of the…

Materials Science · Physics 2016-01-22 Chang-Eun Kim , Jonathan M. Skelton , Aron Walsh , Aloysius Soon

The structural features of the interface between the cystalline and amorphous phases of Si solid are studied in simulations based on a combination of empirical interatomic potentials and a nonorthogonal tight-binding model. The…

Materials Science · Physics 2009-10-31 N. Bernstein , M. J. Aziz , E. Kaxiras

Synthesis of transition metal oxides by microwave irradiation is a faster and energy-saving method compared to conventional heating in an electrical furnace because microwave energy is directly converted into heat within precursors.…

Materials Science · Physics 2024-01-09 Marimuthu Manikandan , Arup Ghosh , Ramanathan Mahendiran
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