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Related papers: Large CaFeAsF single crystals of high quality grow…

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High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…

Superconductivity · Physics 2015-07-03 Yonghui Ma , Hui Zhang , Bo Gao , Kangkang Hu , Qiucheng Ji , Gang Mu , Fuqiang Huang , Xiaoming Xie

Millimeter sized single crystals of CaFe$_{1-x}$Co$_x$AsF were grown using a self-flux method. It is found that high-quality single crystals can be grown from three approaches with different initial raw materials. The chemical compositions…

Superconductivity · Physics 2016-08-09 Yonghui Ma , Kangkang Hu , Qiucheng Ji , Bo Gao , Hui Zhang , Gang Mu , Fuqiang Huang , Xiaoming Xie

We report a simple, reliable method to grow high quality BaFe$_{2-x}$Co$_x$As$_2$ single crystal samples without using any fluxing agent. The starting materials for the single crystal growth come from well-crystallized polycrystalline…

Superconductivity · Physics 2011-03-23 Changjin Zhang , Lei Zhang , Chuanying Xi , Langsheng Ling , Shun Tan , Yuheng Zhang

Measurements of the anisotropic properties of single crystals play a crucial role in probing the physics of new materials. Determining a growth protocol that yields suitable high-quality single crystals can be particularly challenging for…

Materials Science · Physics 2017-06-20 W. R. Meier , T. Kong , S. L. Bud'ko , P. C. Canfield

Self-nucleation in CdZnTe crystal growth remains a significant challenge, despite numerous attempts to achieve large-grain single crystals by restricting multi-nucleation during growth process using the traveling heater method. In this…

Co-doped iron arsenic single crystal of BaFe1.87Co0.13As2 with dimension up to 20 x 10 x 2 mm3 were grown by a nucleation pole: an alumina stick served as nucleation center during growth. The high quality of crystalline was illustrated by…

Superconductivity · Physics 2015-05-13 D. L. Sun , Y. Liu , J. T. Park , C. T. Lin

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

Superconductivity · Physics 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

CuFeO$_2$ single crystals up to 50 mm in length and up to 10 mm in diameter were grown by the optical floating-zone method. Stoichiometric polycrystalline rods with a diameter of 6-12 mm were used as feed materials to produce crystals of…

Materials Science · Physics 2020-01-07 Nora Wolff , Tobias Schwaigert , Dietmar Siche , Darrell G. Schlom , Detlef Klimm

Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…

Superconducting whisker like and bulk single crystals of PrFeAs(O,F) were grown at 3 GPa and 1500 C from NaAs flux using the cubic anvil high pressure and high temperature technique. The ribbon shaped whisker like crystals were 400-1300…

Superconductivity · Physics 2013-11-08 N. D. Zhigadlo

We report the optimized conditions for growing the high quality single crystals of candidate quantum spin-ice Pr2Hf2O7 using the optical floating-zone method. Large single crystals of Pr2Hf2O7 have been grown under different growth…

Strongly Correlated Electrons · Physics 2019-01-02 V. K. Anand , A. T. M. N. Islam , A. Samartzis , J. Xu , N. Casati , B. Lake

A new approach to grow FeSe1-xTex single crystals with optical zone-melting technique was successfully employed. Crystals with actual composition 0.4 < x < 1.0 all show high crystallinity with no phase separation. The ability to visually…

Superconductivity · Physics 2009-11-16 K. W. Yeh , C. T. Ke , T. W. Huang , T. K. Chen , Y. L. Huang , P. M. Wu , M. K. Wu

Millimeter-sized single crystals of LaFeAsO, LaFeAsO1-xFx, and LaFe1-xCoxAsO were grown in NaAs flux at ambient pressure. The detailed growth procedure and crystal characterizations are reported. The as-grown crystals have typical…

Single crystals of Ba0.6K0.4Fe2As2 with excellent quality have been successfully grown without fluxing agent through a simple one-step method for the first time. X-ray diffraction patterns demonstrate that the samples have high crystalline…

Superconductivity · Physics 2015-05-20 Chunlei Wang , Chao Yao , Lei Wang , Yanpeng Qi , Zhaoshun Gao , Dongliang Wang , Xianping Zhang , Yanwei Ma

Incorporation of $\mathrm{Al_{y}Ga_{1-y}N}$ (AGN) semiconductors into high power electronics offers efficiency improvements in power transmission, generation, and use, if approaches to eliminate the defects arising from film-lattice…

A description is given of the traveling solvent technique, which has been used for the crystal growth of both congruently and incongruently melting materials of many classes of intermetallic, chalcogenide, semiconductor and oxide materials.…

Materials Science · Physics 2016-05-13 S. M. Koohpayeh

We grew (Hg,Re)Ba$_2$Ca$_2$Cu$_3$O$_{8+\delta}$ ((Hg,Re)1223) single crystals with good reproducibility via the single-step flux method using monoxides as raw materials. A double-sealing method using a thick-walled quartz tube and a…

We have grown underdoped (x = 0.11, 0.12) and optimally doped (x = 0.16) La2-xSrxCuO4 (LSCO) crystals by traveling-solvent floating-zone (TSFZ) technique. In order to obtain LSCO single crystals of high quality, we have made much effort to…

Superconductivity · Physics 2009-01-23 Xiaoli Shen , Zhengcai Li , Caixia Shen , Wei Lu , Xiaoli Dong , Fang Zhou* , Zhongxian Zhao

MgO single crystals with diameters between 3.5 and 5 mm and lengths up to 40 mm were grown by the optical floating zone technique (OFZ). Despite challenging material properties such as the high melting point of 2825 {\deg}C, very high…

Single crystals of A$_{1-x}$K$_x$Fe$_2$As$_2$ (A=Ba, Sr) with high quality have been grown successfully by FeAs self-flux method. The samples have sizes up to 4 mm with flat and shiny surfaces. The X-ray diffraction patterns suggest that…

Superconductivity · Physics 2009-11-13 Huiqian Luo , Zhaosheng Wang , Huan Yang , Peng Cheng , Xiyu Zhu , Hai-Hu Wen
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