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A detailed high pressure study is carried out on 1T$^\prime$ MoTe$_{2}$ using X-ray diffraction(XRD) and Raman spectroscopy measurements upto about 30.5 GPa. High pressure XRD measurements show no structural transition. All the lattice…

Materials Science · Physics 2020-01-07 Bishnupada Ghosh , Pinku Saha , Goutam Dev Mukherjee

Solid CS$_{2}$ is superficially similar to CO$_{2}$, with the same $Cmca$ molecular crystal structure at low pressures, which has suggested similar phases also at high pressures. We carried out an extensive first principles evolutionary…

Materials Science · Physics 2015-06-23 S. Shahab Naghavi , Yanier Crespo , Roman Martonak , Erio Tosatti

Compositionally tunable vanadium oxyhydrides Sr2VO4-xHx (x = 0 - 1) without considerable anion vacancy were synthesized by high-pressure solid state reaction. The crystal structures and their properties were characterized by powder neutron…

The structural and vibrational properties of phenanthrene are measured at high pressures up to 30.2 GPa by Raman spectroscopy and synchrotron x-ray diffraction techniques. Two phase transitions are observed in raman spectra under pressures…

We have studied dense hydrogen and deuterium experimentally up to 320 GPa and using ab initio molecular dynamic (MD) simulations up to 370 GPa between 250 and 300 K. Raman and optical absorption spectra show significant anharmonic and…

The high-pressure crystal structure evolution of CH3NH3PbBr3 (MAPbBr3) perovskite has been investigated by single-crystal X-ray diffraction and synchrotron-based powder X-ray diffraction. Single-crystal X-ray diffraction reveals that the…

In-situ high pressure single crystal X-ray diffraction study reveals that the quantum material CaMn$_2$Bi$_2$ undergoes a unique plane to chain structural transition between 2 and 3 GPa, accompanied by a large volume collapse. CaMn2Bi2…

Materials Science · Physics 2019-07-18 Xin Gui , Gregory J. Finkelstein , Keyu Chen , Tommy Yong , Przemyslaw Dera , Jinguang Cheng , Weiwei Xie

The effects of pressure on the crystal structure of the three known polymorphs of magnesium sulfate have been theoretically study by means of DFT calculations up to 45 GPa. We determined that at ambient conditions gamma MgSO4 is an unstable…

Materials Science · Physics 2017-05-31 A. Benmakhlouf , D. Errandonea , M. Bouchenafa , S. Maabed , A. Bouhemadou , A. Bentabet

Negative thermal expansion (NTE) materials possess a low-density, open structure which can respond to high pressure conditions, leading to new compounds and/or different physical properties. Here we report that one such NTE material --…

Materials Science · Physics 2016-11-27 Tamas Varga , J. F. Mitchell , Jun Wang , Lindsay G. Arnold , Brian H. Toby , Christos D. Malliakas

In this paper we provide an accurate high-pressure structural and optical study of MAPbI3 hybrid perovskite. Structural data show the presence of a phase transition towards an orthorhombic structure around 0.3 GPa followed by full…

The effects of high pressure on the crystal structure of orthorhombic (Pnma) perovskite type cerium scandate have been studied in situ under high pressure by means of synchrotron x-ray powder diffraction, using a diamond anvil cell. We have…

The orthovanadates are useful as host matrices for immobilization of radioactive wastes. The thermodynamic stability of these materials is crucial for their applications in high pressure and temperatures environment. It is necessary to…

Materials Science · Physics 2019-05-01 R. Mittal , M. K. Gupta , Baltej Singh , L. Pintschovius , Yu D. Zavartsev , S. L. Chaplot

We studied the high-pressure effects on the crystalline structure of monoclinic HfTiO4 and ZrTiO4. We found that the compressibility of these ceramics is highly non-isotropic, being the b-axis the most compressible one. In addition, the…

Materials Science · Physics 2010-09-23 Daniel Errandonea , David Santamaria-Perez , Tatiana Bondarenko , Oleg Khyzhun

Most transition-metal trihalides are dimorphic. The representative chromium-based triad, CrCl3, CrBr3, CrI3, is characterized by the low-temperature phase adopting the trigonal BiI3 type while the structure of the high-temperature phase is…

We report high-pressure x-ray diffraction experiments on BiFeO3 (BFO) single crystals in diamond-anvil cells up to 14 GPa. Two data sets are compared, one in hydrostatic conditions, with helium used as pressure-transmitting medium, and the…

Materials Science · Physics 2011-05-16 Mael Guennou , Pierre Bouvier , Raphaël Haumont , Gaston Garbarino , Jens Kreisel

Using in-situ angle dispersive x-ray diffraction, we have shown that barium tungstate, which exists in scheelite phase at ambient conditions, transforms to a new phase about seven giga pascal. Analysis of our data based on Le bail…

Materials Science · Physics 2009-11-10 Vinod Panchal , Nandini Garg , A. K. Chauhan , Sangeeta , Surinder M. Sharma

We report a room-temperature optical reflectivity study performed on [112]-oriented Cd$_3$As$_2$ single crystals over a broad energy range under external pressure up to 10 GPa. The abrupt drop of the band dispersion parameter…

Materials Science · Physics 2018-05-23 E. Uykur , R. Sankar , D. Schmitz , C. A. Kuntscher

We show that Rb_4C_60 transforms from its ambient pressure orientationally disordered tetragonal structure to an ordered orthorhombic structure (isostructural to Cs_4C_60) at or above 0.4 GPa. This opens the possibility of studying the…

Strongly Correlated Electrons · Physics 2007-05-23 Ashfia Huq , Peter W. Stephens

The crystal structure of the layered, perovskite-related LaTiO_3.41 (La_5Ti_5O_{17+\delta}) has been studied by synchrotron powder x-ray diffraction under hydrostatic pressure up to 27 GPa (T = 295 K). The ambient-pressure phase was found…

Strongly Correlated Electrons · Physics 2007-05-23 I. Loa , K. Syassen , X. Wang , F. Lichtenberg , M. Hanfland , C. A. Kuntscher

(MgFe)O is a solid solution with ferrous iron undergoing the high to low spin state (HS-LS) crossover under high pressure. The exact state of the material in the region of the crossover is still a mystery, as domains with different spin…

Materials Science · Physics 2020-05-20 Konstantin Glazyrin , Saiana Khandarkhaeva , Leonid Dubrovinsky , Michael Sprung
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