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During past years, a number of reports have been published on synthesis of tetragonal allotrope of boron, t-B52 phase. However, no unambiguous characterization of the crystal structure has been performed to the present time, while…

Materials Science · Physics 2013-02-20 Oleksandr O. Kurakevych , Vladimir L. Solozhenko

X-ray and neutron powder diffraction data as a function of temperature are analyzed for the colossal dielectric constant material CaCu3Ti4O12. The local structure is studied using atomic pair distribution function analysis. No evidence is…

Materials Science · Physics 2009-11-10 E. S. Bozin , V. Petkov , P. W. Barnes , P. M. Woodward , T. Vogt , S. D. Mahanti , S. J. L. Billinge

We report the growth of mm-sized Pmnb-Li2FeSiO4 single crystals by means of the optical floating-zone method at high argon pressure and describe the conditions required for a stable growth process. The crystal structure is determined and…

UTe2 is a newly-discovered unconventional superconductor wherein multicomponent topological superconductivity is anticipated based on the presence of two superconducting transitions and time-reversal symmetry breaking in the superconducting…

Superconductivity · Physics 2022-06-02 P. F. S. Rosa , A. Weiland , S. S. Fender , B. L. Scott , F. Ronning , J. D. Thompson , E. D. Bauer , S. M. Thomas

In this work we investigated the temperature dependence of the upper critical field u0Hc2(T) of Fe1.02(3)Te0.61(4)Se0.39(4) and Fe1.05(3)Te0.89(2)Se0.11(2) single crystals by measuring the magnetotransport properties in stable dc magnetic…

Superconductivity · Physics 2010-03-23 Hechang Lei , Rongwei Hu , E. S. Choi , J. B. Warren , C. Petrovic

The correlation between electronic and crystal structures of 1T-TiSe2 in the charge density wave (CDW) state is studied by x-ray diffraction. Three families of reflections are used to probe atomic displacements and the orbital asymmetry in…

CaFe2As2 single crystals under uniaxial pressure applied along the c axis exhibit the coexistence of several structural phases at low temperatures. We show that the room-temperature tetragonal phase is stabilized at low temperatures for…

We have determined the resistive upper critical field Hc2 for single crystals of the superconductor Fe1.11Te0.6Se0.4 using pulsed magnetic fields of up to 60T. A rather high zero-temperature upper critical field of mu0Hc2(0) approx 47T is…

Superconductivity · Physics 2010-01-29 M. H. Fang , J. H. Yang , F. F. Balakirev , Y. Kohama , J. Singleton , B. Qian , Z. Q. Mao , H. D. Wang , H. Q. Yuan

Magnetic structure of tetragonal UAu$_2$Si$_2$ was investigated by single-crystal neutron diffraction experiments. Below $T_{\rm N}$ = 20 K it orders antiferromagnetically with a propagation vector of $k = (2/3, 0, 0)$ and magnetic moments…

Structural, magnetic, electrical transport, and heat capacity data are reported for single crystals of TlFe1.6Se2. This compound crystallizes in a tetragonal structure similar to the ThCr2Si2 structure, but with vacancies in the Fe layer.…

Herein we report on the thermal expansions and temperature-dependent crystal structures of select ternary carbide MAX phases in the Ti-Al-C phase diagram in the 100-1000 deg C temperature range. A bulk sample containing 38 wt.% Ti5Al2C3,…

Materials Science · Physics 2015-06-15 Nina J. Lane , Sven C. Vogel , El'ad N. Caspi , Michel W. Barsoum

The crystal structures of potassium and cesium bistrifluoroacetates were determined at room temperature and at 20 K and 14 K, respectively, with the single crystal neutron diffraction technique. The crystals belong to the I2/a and A2/a…

Chemical Physics · Physics 2015-05-13 A. Cousson , J. F. R. Archilla , J. Tomkinson , F. Fillaux

F-substituted NdOBiS2 superconducting single crystals were grown using CsCl/KCl flux. This is the first example of the single-crystal growth of a BiS2-based superconductor. The obtained single crystals had a plate-like shape with a size of…

We have performed powder neutron diffraction on the new superconductor, CeNi$_{0.8}$Bi$_2$ with a superconducting transtion temperature $T_\textrm{c} \sim$ 4.2 K. The structural parameters of this compound at room temperature are determined…

Superconductivity · Physics 2015-05-27 K. Kodama , S. Wakimoto , N. Igawa , S. Shamoto , H. Mizoguchi , H. Hosono

Heat capacity, magnetic susceptibility, NMR, and resistivity of SrNi2P2 single crystals are presented, illustrating a purely structural transition at 325 K with no magnetism. Bulk superconductivity is found at 1.4 K. The magnitude of the…

Superconductivity · Physics 2009-04-13 F. Ronning , E. D. Bauer , T. Park , S. -H Baek , H. Sakai , J. D. Thompson

Single crystals of EuPd$_3$Si$_2$ were grown using a high-temperature EuPd-flux method. The material was structurally and chemically characterized by single-crystal x-ray diffraction, powder x-ray diffraction, Laue method and…

Strongly Correlated Electrons · Physics 2026-02-19 Michelle Ocker , Franziska Walther , Nour Maraytta , Matthieu Le Tacon , Michael Merz , Cornelius Krellner , Kristin Kliemt

The crystal structure of SmFeAsO has been investigated by means of Rietveld refinement of high resolution synchrotron powder diffraction data collected at 300 K and 100 K. The compound crystallizes in the tetragonal P4/nmm space group at…

Superconductivity · Physics 2022-11-30 A. Martinelli , A. Palenzona , C. Ferdeghini , M. Putti , E. Emerich

The crystal structure, superconducting properties, and electronic structure of a novel superconducting 122-type antimonide, BaPt$_2$Sb$_2$, have been investigated by measurements of powder X-ray diffraction patterns, electrical resistivity,…

La$_{0.4}$Na$_{0.6}$Fe$_2$As$_2$ single crystals have been grown out of an NaAs flux in an alumina crucible and characterized by measuring magnetic susceptibility, electrical resistivity, specific heat, as well as single crystal x-ray and…

A two dimensional crystalline layer is found at the surface of the liquid eutectic Au$_{82}$Si$_{18}$ alloy above its melting point $T_M=359 ^{\circ}$C. Underlying this crystalline layer we find a layered structure, 6-7 atomic layers thick.…