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We have grown cubic centimetre-size crystals of YBa2Cu3Ox suitable for neutron studies, by a top-seeded melt-growth technique. Growth conditions were optimized with an eye toward maximizing phase purity. It was found that the addition of 2%…

Materials identification and structural understanding from powder X-ray diffraction (PXRD) data is a long-standing challenge in materials science, fundamental to discovering and characterizing novel materials. A prerequisite for full…

We describe a new method of 3D image reconstruction of neutron sources that emit correlated gammas (e.g. Cf-252, Am-Be). This category includes a vast majority of neutron sources important in nuclear threat search, safeguards and…

Data Analysis, Statistics and Probability · Physics 2017-01-18 Mateusz Monterial , Peter Marleau , Sara A. Pozzi

A new instrument for spot profile analysis of electron diffraction - SPA-LEED - has been set up. The instrument works either with a transparent phosphor screen for visual inspection of the pattern or in its main mode with a channeltron for…

Materials Science · Physics 2015-01-30 U. Scheithauer , G. Meyer , M. Henzler

Spectra of ultracold neutrons that appeared in experiments on neutron diffraction by a moving grating were measured using the time-of-flight Fourier spectrometer. Diffraction lines of five orders were observed simultaneously. The obtained…

A recent polarized neutron diffraction experiment on the 5d2 rhenium double perovskite Ba2YReO6 held at a low temperature uncovered weak magnetic diffraction peaks. Data analysis inferred a significantly reduced Re dipole moment, and…

Strongly Correlated Electrons · Physics 2021-03-24 S. W. Lovesey , D. D. Khalyavin , G. van der Laan , G. J. Nilsen

When calculating residual strain via neutron or X-ray diffraction, uncertainties propagated from the peak fit are often inadequate to describe the true scatter of measurements about a singular strain state, such as one that should describe…

Materials Science · Physics 2026-05-07 Cole Franz , Michael B. Prime , Jeffrey Bunn , Andrew Payzant , Katharine Page

Local magnetic order and anisotropy are often central for understanding fundamental behavior and emergent functional properties in quantum materials and beyond. Advances in neutron powder diffraction experiments and analysis tools now allow…

Strongly Correlated Electrons · Physics 2025-04-17 Raju Baral , Danielle R. Yahne , Malcolm J. Cochran , Matthew Powell , Joseph W. Kolis , Haidong Zhou , Stuart Calder

In-situ X-ray diffraction (XRD) and transmission electron microscopy (TEM) have been used to investigate many physical science phenomena, ranging from phase transitions, chemical reaction and crystal growth to grain boundary dynamics. A…

In this paper, we propose an advanced methodology for the detection of 3D objects and precise estimation of their spatial positions from a single image. Unlike conventional frameworks that rely solely on center-point and dimension…

Computer Vision and Pattern Recognition · Computer Science 2024-01-04 Dhyey Manish Rajani , Surya Pratap Singh , Rahul Kashyap Swayampakula

Three-dimensional electron diffraction (3D ED) has emerged as a powerful method for solving the structures of sub-micron-sized particles down to nanoparticles. However, it faces technical challenges when applied to beam-sensitive samples or…

This study entailed the successful deployment of a novel neutron interferometer that utilizes multilayer mirrors. The apparatus facilitates a precise evaluation of the wavelength dependence of interference fringes utilizing a pulsed neutron…

We solve the orientation recovery of a tumbling protein in the gas phase from single-event measurements of the spatial positions of its ions after an X-ray laser induced explosion. We simulate diffracted X-ray signal and ion dynamics under…

Chemical Physics · Physics 2026-03-26 Tomas André , Alfredo Bellisario , Nicusor Timneanu , Carl Caleman

Precession of a converged beam during acquisition of a 4D-STEM dataset improves strain, orientation, and phase mapping accuracy by averaging over continuous angles of illumination. Precession experiments usually rely on integrated systems,…

Instrumentation and Detectors · Physics 2025-10-20 Stephanie M. Ribet , Rohan Dhall , Colin Ophus , Karen C. Bustillo

We consider a method of high-fidelity, spatially resolved position measurement of ultracold atoms in an optical lattice. We show that the atom-number distribution can be nondestructively determined at a spatial resolution beyond the…

Quantum Gases · Physics 2015-08-28 Yuto Ashida , Masahito Ueda

The ability to characterise the three-dimensional microstructure of multiphase materials is essential for understanding the interaction between phases and associated materials properties. Here, laboratory-based diffraction-contrast…

Quantification of microstructures is crucial for understanding processing-structure and structure-property relationships in polycrystalline materials. Delineating grain boundaries in bright-field transmission electron micrographs, however,…

Localization of networked nodes is an essential problem in emerging applications, including first-responder navigation, automated manufacturing lines, vehicular and drone navigation, asset navigation and tracking, Internet of Things and 5G…

Networking and Internet Architecture · Computer Science 2023-10-04 Nakul Garg , Irtaza Shahid , Ramanujan K Sheshadri , Karthikeyan Sundaresan , Nirupam Roy

A time-of-flight device was developed to characterize wavelength distribution and uniformity of a cold neutron beam. This device is very compact -- the distance of flight is $60$ cm -- but achieves very high resolution -- the intrinsic…

Three dimensional difference pair distribution functions from X-ray and neutron diffraction experiments are reported for yttria stabilized zirconia (Zr$_{0.82}$Y$_{0.18}$O$_{1.91}$). We use a quantitative analysis of the signatures in the…

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