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A deep learning model is employed to address the challenging problem of V2O5 nanoparticle segmentation and the correlation between the chemical composition and the geometrical features of lithiated V2O5 nanoparticles as an exemplar of a…

Amorphous chalcogenide thin film deposition can be achieved by a spin-coating technique from proper solutions of the corresponding glass. Films produced in this way exhibit certain grain texture, which is presumably related to the cluster…

Materials Science · Physics 2008-03-28 T. Kohoutek , T. Wagner , M. Frumar , A. Chrissanthopoulos , O. Kostadinova , S. N. Yannopoulos

In this paper we present the results of the synthesis and characterisation of nanocrystalline La1-xNaxMnO3+delta samples. Two synthetic routes were employed: polyacrylamide-based sol-gel and propellant synthesis. Pure, single phase…

Materials Science · Physics 2007-05-23 Lorenzo Malavasi , Maria C. Mozzati , Stefano Polizzi , Carlo B. Azzoni , Giorgio Flor

First thermoelectric properties measurements on bulk nanostructured Ba8Ga16Ge30 clathrate-I are presented. A sol-gel-calcination route was developed for preparing amorphous nanosized precursor oxides. The further reduction of the oxides led…

Thin films of perovskite manganite La$_{0.7}$Ca$_{0.3}$MnO$_{3}$ were grown epitaxially on various substrates by either the pulsed laser deposition method or laser molecular beam epitaxy. The substrates change both the volume and symmetry…

Strongly Correlated Electrons · Physics 2009-11-07 J. H. Song , J. H. Park , Y. H. Jeong , T. Y. Koo

Electrochemical devices such as solid oxide fuel cells (SOFC) may greatly benefit from the implementation of nanoengineered thin-film multifunctional layers providing, alongside enhanced electrochemical activity, improved mechanical, and…

Hybrid nanoparticles allow exploiting the interplay of confinement, proximity between different materials and interfacial effects. However, to harness their properties an in-depth understanding of their (meta)stability and interfacial…

Rigid, cage-like molecules, like diamondoids, show unique self-assembly behavior, such as templating 1-D nanomaterial assembly via pathways that are typically blocked for such bulky substituents. We investigate molecular forces between…

Materials Science · Physics 2020-10-30 Ella M. King , Matthew A. Gebbie , Nicholas A. Melosh

Layered LiMnO$_2$ and Li$_2$MnO$_3$ are of great interest for lithium-ion battery cathodes because of their high theoretical capacities. The practical application of these materials is, however, limited due to poor electrochemical…

Materials Science · Physics 2015-02-25 Khang Hoang

We report that the sample miniaturization of first-order-phase-transition bulk systems causes a greater degree of supercooling. From a theoretical perspective, the size effects can be rationalized by considering two mechanisms: (i) the…

Strongly Correlated Electrons · Physics 2018-02-28 H. Oike , M. Suda , M. Kamitani , A. Ueda , H. Mori , Y. Tokura , H. M. Yamamoto , F. Kagawa

The solidification behaviour of suspensions of alumina particles during directional solidification is investigated here by in situ observations using X-ray radiography and tomography. The objective of this study is to assess the influence…

Microwave-assisted hydrothermal synthesis was used to grow LiMnPO$_4$ micro- and nanocrystals from acetate precursors. By appropriate adjustment of the precursor concentration and the pH-value of the reactant, the product composition and…

Materials Science · Physics 2014-05-29 Christoph Neef , Carsten Jähne , Hans-Peter Meyer , Rüdiger Klingeler

This work reports a simple, novel, cost effective and eco-friendly electrolytic synthesis of silver nanoparticles using AgNO3 as metal precursor. The synthesis rate is much faster than other methods and this approach is suitable for large…

General Physics · Physics 2011-11-02 T. Theivasanthi , M. Alagar

In this study, we investigate the magnetic and magnetocaloric properties of nanostructured La0.6Sr0.4CoO3 (LSC) samples synthesized under confinement conditions within porous templates. Using this method, we obtained de-agglomerated…

Cold spray (CS) has emerged as an important additive manufacturing technology over the past decade. This study investigates the effect of oxide layers on the CS process, focusing on the deformation behavior of copper (Cu) and iron (Fe)…

Applied Physics · Physics 2024-08-16 Baihua Ren , Jun Song

Machine learning has emerged as a potent computational tool for expediting research and development in solid oxide fuel cell electrodes. The effective application of machine learning for performance prediction requires transforming…

Materials Science · Physics 2025-03-19 Maksym Szemer , Szymon Buchaniec , Tomasz Prokop , Grzegorz Brus

The short diffusion lengths in insertion battery nanoparticles render the capacitive behavior of bounded diffusion, which is rarely observable with conventional larger particles, now accessible to impedance measurements. Coupled with…

Chemical Physics · Physics 2012-05-31 J. Song , M. Z. Bazant

The properties of silver nanoparticles (AgNPs) are affected by various parameters, making optimisation of their synthesis a laborious task. This optimisation is facilitated in this work by concurrent use of a T-junction microfluidic system…

The separation of liquid mixture components is relevant to many applications -- ranging from water purification to biofuel production -- and is a growing concern related to the UN Sustainable Development Goals (SDGs), such as ``Clean water…

Mesoscale and Nanoscale Physics · Physics 2023-04-21 Roger Bellido-Peralta , Fabio Leoni , Carles Calero , Giancarlo Franzese

Solid electrolytes for solid-state Li-ion batteries are stimulating considerable interest for next-generation energy storage applications. The Li$_7$La$_3$Zr$_2$O$_{12}$ garnet-type solid electrolyte has received appreciable attention as a…

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