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Under high pressure conditions, Zr undergoes a phase transformation from its ambient equilibrium hexagonal close packed $\alpha$ phase to hexagonal $\omega$ phase. Upon returning to ambient conditions, the material displays hysteretic…

Sintered samples of monoclinic zirconia (alpha-ZrO2) have been irradiated at room temperature with 6.0-GeV Pb ions in the electronic slowing down regime. X-ray diffraction (XRD) and micro-Raman spectroscopy measurements showed unambiguously…

Materials Science · Physics 2016-08-16 Jean-Marc Costantini , Andrée Kahn-Harari , Francois Beuneu , François Couvreur

We study the thermally activated, slow conversion of the hysteretically retained $\omega$ phase into stable $\alpha$ phase in recovered samples of shocked zirconium. The $\omega$-phase decays in time following an algebraic law, unlike the…

Materials Science · Physics 2015-10-05 Cristiano Nisoli , Honxiang Zong , Stephen R. Niezgoda , Donald W. Brown , Turab Lookman

We present results from ramp compression experiments on high-purity Zr that show the $\alpha \rightarrow \omega$, $\omega \rightarrow \beta$, as well as reverse $\beta \rightarrow \omega$ phase transitions. Simulations with a multi-phase…

Materials Science · Physics 2022-05-25 C. W. Greeff , J. Brown , N. Velisavljevic , P. A. Rigg

The accurate prediction of solid-solid structural phase transitions at finite temperature is a challenging task, since the dynamics is so slow that direct simulations of the phase transitions by first-principles (FP) methods are typically…

Materials Science · Physics 2021-05-25 Peitao Liu , Carla Verdi , Ferenc Karsai , Georg Kresse

This study examines the phase transitions occurring during linear heating of the Zr15Nb alloy through a comprehensive, multi-technique methodology comprising in-situ high-energy synchrotron X-ray diffraction (HEXRD), electrical resistance…

The first study of the effect of the initial microstructure on its evolution under hydrostatic compression before, during, and after the irreversible $\alpha\rightarrow\omega$ phase transformation and during pressure release in Zr using in…

Materials Science · Physics 2024-02-23 K. K. Pandey , Valery I. Levitas , Changyong Park , Guoyin Shen

Phase transitions in metastable $\alpha$-, $\kappa(\epsilon)$-, and $\gamma$-Ga$_2$O$_3$ films to thermodynamically stable $\beta$-Ga$_2$O$_3$ during annealing in air, N$_2$, and vacuum have been systematically investigated via in-situ…

Materials Science · Physics 2024-05-02 J. Tang , K. Jiang , P. Tseng , R. C. Kurchin , L. M. Porter , R. F. Davis

The elasticity, dynamic properties, and superconductivity of $\alpha$, $\omega$, and $\beta$ Zr are investigated by using first-principles methods. Our calculated elastic constants, elastic moduli, and Debye temperatures of $\alpha$ and…

Materials Science · Physics 2015-05-19 Bao-Tian Wang , Peng Zhang , Han-Yu Liu , Wei-Dong Li , Ping Zhang

We present a kinetic model for solid state phase transformation (alpha<-->beta) of common zirconium alloys used as fuel cladding material in light water reactors. The model computes the relative amounts of beta or alpha phase fraction as a…

Materials Science · Physics 2021-04-01 A. R. Massih , L. O. Jernkvist

An in-situ neutron diffraction investigation of the annealing and healing of dislocations in the bulk Pd-D2 system was carried out. Lattice misfit between the alpha and beta hydride phases produces dislocations during the phase transition…

Materials Science · Physics 2022-05-02 T. A. Webb , C. J. Webb , E. MacA. Gray

The overall solid-to-solid phase transformation kinetics under non-isothermal conditions has been modeled by means of a differential equation method. The method requires provisions for expressions of the fraction of the transformed phase in…

Materials Science · Physics 2015-05-13 Ali R. Massih , Lars O. Jernkvist

Controlled mechanical loading was applied to Ti-15Mo alloy during annealing at 550 $^\circ$C. Massive formation of the $\omega_{\textrm{iso}}$ phase from the parent $\beta$-phase occurred during annealing at 550 $^\circ$C without external…

SrAl2Si2 crystallizes into either a semimetallic, CaAl2Si2-type, \alpha phase or a superconducting, BaZn2P2-type, \beta phase. We explore possible \alpha --Pc;Tc--> \beta transformations by employing pressure- and temperature-dependent…

The effect of increasing temperature on the structural stability and interactions of two kinds of Al/Zr (Al(1%wtSi)/Zr and Al(Pure)/Zr) multilayer mirrors are investigated. All Al/Zr multilayers annealed from 200^{\circ}C to 500^{\circ}C,…

Materials Science · Physics 2015-06-11 Qi Zhong , Shuang Ma , Zhong Zhang , Runze Qi , Jia Li , Zhanshan Wang , Philippe Jonnard

This study demonstrates that a space charge layer is formed on dislocation during mechanical deformation at elevated temperature. High density of dislocation lines is generated in bulk single crystalline Y2O3 stabilized ZrO2 (YSZ) by…

Materials Science · Physics 2020-03-24 Kyoung-Won Park

In {\delta}-Ag2/3V2O5 with charge degrees of freedom in V, it is known that the charge ordering state and physical properties of V that appear at low temperatures depend strongly on the ordering state of Ag. In this study, we focused on the…

Strongly Correlated Electrons · Physics 2024-03-13 T. Kubo , K. Kojima , N. Katayama , T. Runčevski , R. E. Dinnebier , A. S. Gibbs , M. Isobe , H. Sawa

A detailed high pressure investigation is carried out using x-ray diffraction, Raman spectroscopy and low temperature resistivity measurements on hexagonal ZrSe$_{2}$ having an excess of 3 at.\% Zr. Structural studies show that the sample…

Strongly Correlated Electrons · Physics 2022-09-21 Bishnupada Ghosh , Mrinmay Sahu , Debabrata Samanta , Pinku Saha , Anshuman Mandal , Goutam Dev Mukherjee

Alloys of hexagonal $\delta$-phase UZr$_2$ have been synthesized and studied by means of heat capacity, magnetic susceptibility, magnetization, electrical resistivity, magnetoresistance, thermoelectric power, thermal conductivity…

Results of X-ray diffraction experiments on solid oxygen at low temperature and at pressures up to 10 GPa are presented.A careful sample preparation and annealing around 240 K allowed to obtain very good diffraction patterns in the…

Materials Science · Physics 2009-11-07 Federico A. Gorelli , Mario Santoro , Lorenzo Ulivi , Michael Hanfland
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