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By varying the parameters controlling the growth of crystals, including the thermodynamic variables, such as temperature, pressure, and reagent composition and the kinetic factors, namely reaction time and cooling rate, we found the most…

Superconductivity · Physics 2019-06-26 Nikolai D. Zhigadlo

Symmetry plays an important role in determining the physical properties in condensed matter physics, as the symmetry operations of any physical property must include the symmetry operations of the point group of the crystal. As a…

Superconductivity · Physics 2024-10-29 Shangfei Wu , Fei-Ting Huang , Xianghan Xu , Ethan T. Ritz , Turan Birol , Sang-Wook Cheong , Girsh Blumberg

We describe the crystal growth of high quality single crystals of the non-centrosymmetric superconductor, Ru7B3 by the floating zone technique, using an optical furnace equipped with xenon arc lamps. The crystals obtained are large and…

Superconductivity · Physics 2014-07-29 Ravi P. Singh , Natalia A. Parzyk , Martin R. Lees , Don McK Paul , Geetha Balakrishnan

We have synthesized polycrystalline samples of the noncentrosymmetric superconductor Mo3Al2C by arc and RF melting, measured its transport, magnetic and thermodynamic properties, and computed its band structure. Experimental results…

NbBiCh$_3$ (Ch = S, Se) misfit-layered superconducting single crystals were successfully grown using a CsCl/KCl flux for the first time. The obtained crystals had a well-developed habit parallel to the c-plane with a typical width of 1-2 mm…

Magneto-transport measurements of Pr$_4$Ni$_3$O$_{10}$ single crystals performed under externally applied pressures up to 73 GPa in diamond anvil cells with either KBr or Nujol oil as pressure media yield signatures of superconductivity…

Electrical resistivity, specific heat and NMR measurements classify non-centrosymmetric $\rm Mo_3Al_2C$ ($\beta$-Mn type, space group $P4_132$) as a strong-coupled superconductor with $T_c = 9$~K deviating notably from BCS-like behaviour.…

Single crystals of A$_{1-x}$K$_x$Fe$_2$As$_2$ (A=Ba, Sr) with high quality have been grown successfully by FeAs self-flux method. The samples have sizes up to 4 mm with flat and shiny surfaces. The X-ray diffraction patterns suggest that…

Superconductivity · Physics 2009-11-13 Huiqian Luo , Zhaosheng Wang , Huan Yang , Peng Cheng , Xiyu Zhu , Hai-Hu Wen

Bulk single crystals of SrPt3P have been grown for the first time by a self-flux method at 2 GPa and 1500 {\deg}C using the cubic-anvil, high-pressure and high-temperature technique. The grown black crystals were found to have either a…

Superconductivity · Physics 2016-10-11 Nikolai D. Zhigadlo

"F-free" CeOBiS$_2$ single crystals have successfully grown, thoroughly eliminating a concern about F-contamination by using a high-purity CsCl flux. The obtained crystals have a plate-like shape with a size of 1.0-3.0 mm in the…

Single crystals of LaNiSb$_3$ were grown using the Sn flux method. Structural characterization confirms that LaNiSb$_3$ crystallizes in the orthorhombic $Pbcm$ space group with lattice parameters $a = 13.0970(2)\,\mathrm{\AA}$, $b =…

Materials Science · Physics 2026-03-24 Haribrahma Singh , Aarti Gautam , Prabuddha Kant Mishra , Rie Y. Umetsu , Ashok Kumar Ganguli

F-substituted NdOBiS2 superconducting single crystals were grown using CsCl/KCl flux. This is the first example of the single-crystal growth of a BiS2-based superconductor. The obtained single crystals had a plate-like shape with a size of…

We report growth of high-quality single crystals of CeCl3 using a modified Bridgman Stockbarger method in an infrared image furnace. The grown crystals are characterized using single-crystal/powder X-ray diffraction, Laue X-ray diffraction,…

Strongly Correlated Electrons · Physics 2024-07-03 Nashra Pistawala , Suman Karmakar , Rajeev Rawat , Surjeet Singh

Single crystals of KOs2O6 have been grown in a sealed quartz ampoule. Detailed single crystal X-ray diffraction studies at room temperature show Bragg peaks that violate Fd-3m symmetry. With a comparative structure refinement the structure…

Superconductivity · Physics 2009-11-11 G. Schuck , S. M. Kazakov , K. Rogacki , N. D. Zhigadlo , J. Karpinski

In a superconductor that lacks inversion symmetry, the spatial part of the Cooper pair wave function has a reduced symmetry, allowing for the mixing of spin-singlet and spin-triplet Cooper pairing channels and thus providing a pathway to a…

[(SnSe)$_{1+\delta}$]$_m$(NbSe$_2$) ($m$ = 1-6, 8, and 12) highly orientated crystals 1-2 mm in size and well-defined c-planes were successfully grown using CsCl/KCl flux, including the first growth of crystals with $m = 12$. The stacked…

We successfully grew the high-quality single crystals of $A_{x}$Fe$_2$Se$_2$ ($A$ = K and Cs) by self-flux method. Sharp superconducting transition was observed for both types of crystals. The crystals show the onset superconducting…

Superconductivity · Physics 2011-07-07 J. J. Ying , X. F. Wang , X. G. Luo , A. F. Wang , M. Zhang , Y. J. Yan , Z. J. Xiang , R. H. Liu , P. Cheng , G. J. Ye , X. H. Chen

We report crystal growth and below 2.5K superconductivity of Nb0.25Bi2Se3. These crystals are grown by self flux method. The X-ray diffraction (XRD) pattern of as grown crystal flake shows (00l) plane (c-orientation) growth. The Rietveld…

Superconductivity · Physics 2019-11-20 M. M. Sharma , P. Rani , Lina Sang , X. L. Wang , V. P. S. Awana

We report on the crystal growth and characterization of ABi3 (A=Ba,Sr) superconductors. Single crystals of both compounds were grown by the self-flux technique. BaBi3 crystallized in a tetragonal structure with space group P4/mmm and SrBi3…

Superconductivity · Physics 2016-07-13 Rajveer Jha , Marcos A. Avila , Raquel A. Ribeiro

Here we report the preparation and superconductivity of the 133-type Cr-based quasi-one-dimensional (Q1D) RbCr3As3 single crystals. The samples were prepared by the deintercalation of Rb+ ions from the 233-type Rb2Cr3As3 crystals which were…

Superconductivity · Physics 2018-01-16 Tong Liu , Qing-Ge Mu , Bo-Jin Pan , Jia Yu , Bin-Bin Ruan , Kang Zhao , Gen-Fu Chen , Zhi-An Ren
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