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We use ultrasensitive electron backscatter diffraction (EBSD) to map the local crystal orientations, grains, and grain boundaries in CH3NH3PbI3 (MAPI) perovskite thin films. Although the true grain structure is broadly consistent with the…

Lattice deformation is a powerful way to engineer the properties of two-dimensional (2D) materials, making their precise measurement an important challenge for both fundamental science and technological applications. Here, we demonstrate…

Materials Science · Physics 2026-02-02 Z. Mu , Z. Zhang , J. Fraunié , C. Robert , G. Seine , B. Gil , G. Cassabois , V. Jacques

Aberration-corrected scanning transmission electron microscopes (STEM) provide sub-angstrom lateral resolution; however, the large convergence angle greatly reduces the depth of field. For microscopes with a small depth of field,…

Materials Science · Physics 2011-12-15 Robert Hovden , Huolin L. Xin , David A. Muller

Broadband longitudinal-to-transverse mode conversion under normal incidence remains difficult to achieve, especially with structurally simple designs. Numerical simulations show that a single periodic row of inclined long-slits near a free…

Applied Physics · Physics 2025-11-26 Kaifei Feng , Weidong Wang , Yucheng Gao , Fengming Liu , Qiujiao Du , Wenshuai Zhang , Pai Peng

Resolving pseudosymmetry has long presented a challenge for electron backscatter diffraction (EBSD) and has been notoriously challenging in the case of tetragonal ZrO2 in particular. In this work, a method is proposed to resolve…

Materials Science · Physics 2020-03-11 Edward L. Pang , Peter M. Larsen , Christopher A. Schuh

The key to most surface phenomenon lies with the surface structure. Particularly it is the charge density distribution over surface that primarily controls overall interaction of the material with external environment. It is generally…

Materials Science · Physics 2025-04-16 Nirman Chakraborty , Swastik Mondal

High-throughput analysis of multidimensional transmission electron microscopy (TEM) datasets remains a significant challenge, limiting the broader impact on strategic materials research. Conventional workflows typically involve sequential,…

Materials Science · Physics 2025-07-16 Arda Genc , Ravit Silverstein

Recent reviews in ultrafast electron diffraction (UED) have claimed that relativistic electrons exhibit enhanced elastic scattering efficiency, frequently quantified as a \gamma^2 increase in the differential cross section. These claims,…

Accelerator Physics · Physics 2025-09-24 Grant Brassem , Christian Viernes , German Sciaini

Electron backscatter diffraction is a powerful tool for mapping crystallographic microstructures. However, the primary crux to improving orientation accuracy and applying the technique to challenging materials lies in the correct…

Materials Science · Physics 2026-04-29 Claire Griesbach , Dennis M. Kochmann

High precision measurements of stellar spectroscopic line profiles and their changes over time contain very valuable information about the physics of the stellar photosphere (stellar activity) and can be used to characterize extrasolar…

Earth and Planetary Astrophysics · Physics 2017-11-08 John B. P. Strachan , Guillem Anglada-Escude

Here we analyze a three-dimensional distribution of crystallographic slip measured in-situ during the uniaxial deformation of hexagonal Ti-7Al. The slip field is reconstructed using a novel methodology that combines spatially resolved…

Materials Science · Physics 2021-04-27 Darren C. Pagan , Kelly E. Nygren , Matthew P. Miller

The Kikuchi bands arise from Bragg diffraction of incoherent electrons scattered within a crystalline specimen and can be observed in both the transmission and reflection modes of scanning electron microscopy (SEM). Converging, rocking, or…

High Dynamic Range (HDR) imaging aims to generate an artifact-free HDR image with realistic details by fusing multi-exposure Low Dynamic Range (LDR) images. Caused by large motion and severe under-/over-exposure among input LDR images, HDR…

Computer Vision and Pattern Recognition · Computer Science 2024-08-30 Shuaikang Shang , Xuejing Kang , Anlong Ming

Techniques for training artificial neural networks (ANNs) and convolutional neural networks (CNNs) using simulated dynamical electron diffraction patterns are described. The premise is based on the following facts. First, given a suitable…

Mesoscale and Nanoscale Physics · Physics 2021-03-08 Renliang Yuan , Jiong Zhang , Lingfeng He , Jian-Min Zuo

In the Cu Cr system, the formation of supersaturated solid solutions can be obtained by severe plastic deformation. Energy dispersive synchrotron diffraction measurements on as deformed Cu Cr samples as a function of the applied strain…

Under white light illumination, gratings produce an angular distribution of wavelengths dependent on the diffraction order and geometric parameters. However, previous studies of gratings are limited to at least one geometric parameter…

Understanding mechanical properties of materials requires not only complete determination of the three-dimensional response at a local scale, but also knowledge of the mode or the mechanism by which deformation takes place. Probing…

Materials Science · Physics 2010-04-28 David Bronfenbrenner , Matthew Bibee , Apurva Mehta

Nanoscale strain mapping by four-dimensional scanning transmission electron microscopy (4D-STEM) relies on determining the precise locations of Bragg-scattered electrons in a sequence of diffraction patterns, a task which is complicated by…

The ability to measure small deformations or strains is useful for understanding many aspects of materials. Here, a new analysis of speckle diffraction peaks is presented in which the systematic shifts of the speckles are analyzed allowing…

Materials Science · Physics 2021-02-17 Mark Sutton , J. R. M. Lhermitte , F. Livet , F. Ehrburger-Dolle

We demonstrate high-resolution non-iterative holographic coherent diffraction imaging with hard X-rays using a novel phase-shifting reference, fabricated by atomic layer deposition to produce nanosharp 3D structure. The method surpasses the…

Mesoscale and Nanoscale Physics · Physics 2016-10-17 Mirna Saliba , Jeroen Bosgra , Christoph Rau , Christian David , Aaron D. Parsons , Ulrich H. Wagner , Pierre Thibault
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