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A Cu-Fe nanocomposite containing 50 nm thick iron filaments dispersed in a copper matrix was processed by torsion under high pressure at various strain rates and temperatures. The resulting nanostructures were characterized by transmission…
To study the size and strain rate dependency of copper polycrystalline microstructures, a multi-layered copper/Al$_2$O$_3$ thin film was deposited on a Si substrate using a hybrid deposition system (combining physical vapour and atomic…
The effect of ultrasonic melting processing on three-dimensional architecture of intermetallic phases and pores in two multicomponent cast Al-5.0Cu-0.6Mn-0.5 Fe alloys is characterized using conventional microscopy and synchrotron X-ray…
We report the synthesis of cobalt nanoparticles with different shapes and sizes by rapid pyrolysis of cobalt carbonyl in the presence of various surfactants. The size and shape of the nanoparticles were influenced by reaction conditions,…
In the present paper we report an in-situ high-energy X-ray diffraction analysis of MgB2 tapes during the preparation process. The experiment was performed in a specifically designed furnace working in reducing atmosphere, compatible with…
Co-reduction of multicomponent oxides with hydrogen provides a carbon-neutral approach toward sustainable alloy design. Herein, we investigate the hydrogen-based direct reduction, using in-situ high-energy X-ray diffraction of two precursor…
The structural and microstructural properties of the Sm(Fe1-xRux)As(O0.85F0.15) system were investigated by means of high-resolution synchrotron X-ray powder diffraction between 10 K and 300 K. The tetragonal to orthorhombic structural…
We report results of 57Fe Mossbauer and 31P NMR studies of a phosphide FeP powder sample performed in a wide temperature range including the point (TN ~ 120 K) of magnetic phase transitions. The 57Fe Mossbauer spectra at low temperatures T…
We prepared very high-coercivity cobalt ferrite nanoparticles using short-time high-energy mechanical milling. After the milling process, the coercivity of the nanoparticles reached 3.75 kOe - a value almost five times higher than that…
Using M\"ossbauer and EPR spectroscopy we have studied the insulating ferromagnetic La$_{1-x}$Ca$_x$Mn$_{0.99}$$^{57}$Fe$_{0.01}$O$_3$ ($x=0.175$) compound prepared in air and reduced atmosphere. The average hyperfine field follows a mean…
The structure of the recently identified metastable ice XVII, obtained by release of hydrogen from the C$_0$ D$_2$O-H$_2$ compound (filled ice), has been accurately measured by neutron powder diffraction. The diffraction pattern is indexed…
The effect of composition on microstructure both at the length scale of the secondary dendrite arm spacing and nano-sized dispersoids during homogenization of Al-Zn-Cu-Mg-Zr alloys has been studied. A comprehensive model that can predict…
The processing of binary alloys consisting of ferromagnetic Fe and antiferromagnetic Cr by severe plastic deformation (SPD) with different chemical compositions has been investigated. Although the phase diagram exhibits a large gap in the…
The structural and magnetic properties of the hexagonal four-layer form of SrMnO$_3$ have been investigated by combining magnetization measurements, electron diffraction and high-resolution synchrotron X-ray and neutron powder diffraction.…
Topologically non trivial spin textures host great promise for future spintronic applications. Skyrmions in particular are of burgeoning interest owing to their nanometric size, topological protection, and high mobility via ultra-low…
We studied the structural and magnetic properties of the solid solution Fe$_{1-x}$Ni$_{x}$B through theoretical and experimental approaches. Powder X-ray diffraction, X-ray Pair Distribution Function analysis, and energy dispersive X-ray…
We investigate the microwave spectra of ultracold alkali metal dimers in magnetic, electric and combined fields, taking account of the hyperfine structure due to the nuclear spins. We consider the molecules 41K87Rb and 7Li133Cs, which are…
LSCF is a promising candidate for the cathode in SOFCs. Understanding the microstructural characteristics is crucial to its application because they predominately determine the performance and durability of the porous cathodes and hence of…
The high-pressure structural behavior of europium orthovanadate has been studied using in-situ, synchrotron based, high-pressure x-ray powder diffraction technique. Angle-dispersive x-ray diffraction measurements were carried out at room…
The ceramic pellets of the nominal compositions Bi$_{0.7}$Ba$_{0.3}$Fe$_{1-x}$Ti$_x$O$_3$ (x = 0.00-0.20) were prepared initially by standard solid state reaction technique. The pellets were then ground into micrometer-sized powders and…