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Altermagnetic properties have been recently proposed in polar magnetic oxides, M$_{2}$Mo$_{3}$O$_{8}$ (M = Mn, Fe, Co, Ni), where improved characteristics of stronger magnetoelectric coupling and higher magnetic transition temperatures were…

The Ho2Ti2O7, Er2Ti2O7 and Yb2Ti2O7 pyrochlores were studied by synchrotron X-ray diffraction to determine whether the (002) peak, forbidden in the pyrochlore space group Fd-3m but observed in single crystal neutron scattering measurements,…

Materials Science · Physics 2015-04-24 Kristen Baroudi , Bruce D. Gaulin , Saul H. Lapidus , R. J. Cava

(Mn,Fe)2(P,Si) single crystals have been successfully grown by flux method. Single crystal diffraction demonstrates that Mn0.83Fe1.17P0.72Si0.28 crystallizes in a hexagonal crystal structure (space group P-62m) at both 100 and 280 K, in the…

Materials Science · Physics 2015-08-03 H. Yibole , F. Guillou , Y. K. Huang , G. R. Blake , A. J. E. Lefering , N. H. van Dijk , E. Brück

Little is so far known about the magnetism of the $\rm A_2B_2O_7$ monoclinic layered perovskites that replace the spin-ice supporting pyrochlore structure for $r_A/r_B>1.78$. We show that high quality monoclinic Pr$_2$Ti$_2$O$_7$ single…

F-substituted NdOBiS2 superconducting single crystals were grown using CsCl/KCl flux. This is the first example of the single-crystal growth of a BiS2-based superconductor. The obtained single crystals had a plate-like shape with a size of…

We report the anisotropic magnetic properties of the ternary compound ErAl$_2$Ge$_2$. Single crystals of this compound were grown by high temperature solution growth technique,using Al:Ge eutectic composition as flux. From the powder x-ray…

Strongly Correlated Electrons · Physics 2020-04-22 Moumita Nandi , A. Thamizhavel , S. K. Dhar

Single crystals of MgB2 with a size up to 1.5x0.9x0.2 mm3 have been grown with a high pressure cubic anvil technique. The crystal growth process is very peculiar and involves an intermediate nitride, namely MgNB9. Single crystals of BN and…

Ni-doped LiMn0.95Ni0.05PO4 single crystals have been grown for the first time by the travelling-solvent floating-zone method at low Argon pressure. The grown sample exhibits large single crystalline grains as revealed by means of…

Single crystals of SmFeAsO1-xFy of a size up to 120 micrometers have been grown from NaCl/KCl flux at a pressure of 30 kbar and temperature of 1350-1450 C using the cubic anvil high-pressure technique. The superconducting transition…

Superconductivity · Physics 2009-11-13 N. D. Zhigadlo , S. Katrych , Z. Bukowski , S. Weyeneth , R. Puzniak , J. Karpinski

Single crystal growth is a widely explored method of synthesizing materials in the solid state. The last few decades have seen significant improvements in the techniques used to synthesize single crystals, but there has been comparatively…

Materials Science · Physics 2022-09-21 Tanya Berry , Nicholas Ng , Tyrel M. McQueen

Single crystals of a new twinned hexagonal perovskite compound Sr8Os6.3O24 have been synthesized, and structural and magnetic properties have been determined. The compound crystallizes in a hexagonal cell with lattice parameters a =…

We present synchrotron x-ray diffraction, neutron powder diffraction and time-of-flight inelastic neutron scattering measurements on the rare earth pyrochlore oxide Nd2Zr2O7 to study the ordered state magnetic structure and cystal field…

Strongly Correlated Electrons · Physics 2016-01-20 J. Xu , V. K. Anand , A. K. Bera , M. Frontzek , D. L. Abernathy , N. Casati , K. Siemensmeyer , B. Lake

We report the synthesis, and structural and physical properties of CaFe4As3 single crystals. Needle-like single crystals of CaFe4As3 were grown out of Sn flux and the compound adopts an orthorhombic structure as determined by X-ray…

Superconductivity · Physics 2015-05-27 A. B. Karki , G. T. McCandless , S. Stadler , Y. M. Xiong , J. Li , Julia Y. Chan , R. Jin

High-quality metallocene single crystals with a low density of impurities and high homogeneity were prepared using the physical vapor transport method. These crystals were then characterized using various spectroscopic tools and X-ray…

We report on the single crystal growth of Eu(Pd$_{1-x}$Au$_x$)$_2$Si$_2$, $0< x\leq 0.2$, from a levitating Eu-rich melt using the Czochralski method. Our structural analysis of the samples confirms the ThCr$_2$Si$_2$-type structure as well…

Experiments and simulations are used to study the kinetics of crystal growth in a mixture of magnetic and nonmagnetic particles suspended in ferrofluid. The growth process is quantified using both a bond order parameter and a mean domain…

Soft Condensed Matter · Physics 2017-01-11 An T. Pham , Ryohei Seto , Johannes Schonke , Daniel Y. Joh , Ashutosh Chilkoti , Eliot Fried , Benjamin B. Yellen

Neutron diffraction studies have been carried out in the applied magnetic field H(//[011]) on a single crystal of pyrochlore ferromagnet Nd2Mo2O7, whose Hall resistivity(r_H) has been reported to have quite unusual magnetic field (H)- and…

Strongly Correlated Electrons · Physics 2009-11-07 Yukio Yasui , Satoshi Iikubo , Hiroshi Harashina , Taketomo Kageyama , Masafumi Ito , Masatoshi Sato , Kazuhisa Kakurai

In this work we present inelastic neutron scattering experiments which probe the single ion ground states of the rare earth pyrochlores $R_2$Ti$_2$O$_7$ ($R$ = Tb, Dy, Ho). Dy$_2$Ti$_2$O$_7$ and Ho$_2$Ti$_2$O$_7$ are dipolar spin ices, now…

Materials Science · Physics 2016-07-26 M Ruminy , E Pomjakushina , K Iida , K Kamazawa , D T Adroja , U Stuhr , T Fennell

We report the low temperature magnetic properties of the pyrochlore Pr$_2$Hf$_2$O$_7$. Polycrystalline and single-crystal samples are investigated using time-of-flight neutron spectroscopy and macroscopic measurements, respectively. The…

The optical floating zone crystal growth technique is a well-established method for obtaining large, high-purity single crystals. While the floating zone method has been constantly evolving for over six decades, the development of…

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