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Single crystals of a novel ruthenate, Ca2Ru2O7, were obtained. An X-ray diffraction study on a single crystal revealed that this material crystallizes in a pyrochlore structure with a lattice parameter, a = 10.197 Angstroms. The magnetic…

Materials Science · Physics 2009-11-11 Taiya Munenaka , Hirohiko Sato

Single crystals of the three-dimensional frustrated magnet and spin liquid candidate compound PbCuTe$_2$O$_6$ were grown using both the Travelling Solvent Floating Zone (TSFZ) and the Top-Seeded Solution Growth (TSSG) techniques. The growth…

Materials Science · Physics 2021-11-25 A. R. N. Hanna , A. T. M. N. Islam , R. Feyerherm , K. Siemensmeyer , K. Karmakar , S. Chillal , B. Lake

The Fe^{4+}-containing cubic perovskite phase SrFeO_3-x is of interest both for its high-temperature, oxygen-conducting properties as a solid oxide fuel cell component, and at low temperatures, where it exhibits a plethora of helical…

Materials Science · Physics 2012-10-23 D. C. Peets , Jung-hwa Kim , M. Reehuis , P. Dosanjh , B. Keimer

Pyrochlore erbium titanate samples in the form of powders (with nominal compositions of Er2Ti2+xO7) and bulk single crystals were prepared to elucidate the effect of synthesis and growth conditions on their composition, structure, and…

Materials Science · Physics 2018-12-14 Q. Wang , A. Ghasemi , A. Scheie , S. M. Koohpayeh

In this letter, we report growth and characterization of bulk Bi2Se3 single crystals. The studied Bi2Se3 crystals are grown by self flux method through solid state reaction from high temperature (950C) melt of constituent elements and slow…

Millimeter sized single crystals of Mo3Sb7 are grown using the self-flux technique and a thorough characterization of their structural, magnetic, thermal and transport properties is reported. The structure parameters for the…

Superconductivity · Physics 2013-05-24 J. -Q. Yan , M. A. McGuire , A. F. May , H. Cao , A. D. Christianson , D. G. Mandrus , B. C. Sales

We report the single crystal growth and anisotropic magnetic properties of the tetragonal RAg$_2$Ge$_2$ (R = Pr, Nd and Sm) compounds which crystallize in the ThCr$_2$Si$_2$ type crystal structure with the space group \textit{I4/mmm}. The…

Strongly Correlated Electrons · Physics 2015-05-13 Devang A. Joshi , R. Nagalakshmi , R. Kulkarni , S. K. Dhar , A. Thamizhavel

Centimeter-sized single crystals of Sr$_{1.5}$La$_{0.5}$RhO$_{4}$ were grown by the floating zone method at oxygen pressures of 20~bar. The quality of our single crystals was confirmed by X-ray Laue, powder and single crystal X-ray…

Strongly Correlated Electrons · Physics 2017-09-06 Z. W. Li , H. Guo , Z. Hu , T. S. Chan , K. Nemkovski , A. C. Komarek

This work presents a comprehensive investigation of the structural, magnetic, and electronic properties of the double perovskite Ba$_2$CoMoO$_6$ (BCMO). Single crystals were grown via floating-zone and Czochralski techniques and…

Strongly Correlated Electrons · Physics 2026-03-17 A. R. N. Hanna , M. M. Ferreira-Carvalho , S. H. Chen , C. F. Chang , C. Y. Kuo , A. T. M. N. Islam , R. Feyerherm , L. H. Tjeng , B. Lake

We report on the growth of stoichiometric Sr$_2$IrO$_4$ single crystals, which allow us to unveil their intrinsic magnetic properties. The effect of different growth conditions has been investigated for crystals grown by the flux method. We…

Strongly Correlated Electrons · Physics 2016-04-27 N. H. Sung , H. Gretarsson , D. Proepper , J. Porras , M. Le Tacon , A. V. Boris , B. Keimer , B. J. Kim

We report on the crystal and magnetic structures, magnetic, and transport properties of SrMnSb$_2$ single crystals grown by the self-flux method. Magnetic susceptibility measurements reveal an antiferromagnetic (AFM) transition at $T_{\rm…

Reliable and profound studies of actual magnetic domain structure in rare-earth A2Ir2O7 pyrochlore iridates are frequently limited by insufficient sample quality or lack of single crystals. We report the magnetic properties of the…

We report the magnetic characterization of the frustrated transition metal pyrochlore NaCaCo$_2$F$_7$. This material has high spin Co$^{2+}$ in CoF$_6$ octahedra in a pyrochlore lattice, and disordered non-magnetic Na and Ca on the…

Materials Science · Physics 2015-06-19 J. W. Krizan , R. J. Cava

Single crystals of SrMn$_2$Ni$_6$Te$_3$O$_{18}$, a member of the ferroaxial-type magnetic oxide family $AB_{2}C_{6}$Te$_3$O$_{18}$ ($A$ = Pb, Sr; $B$ = Mn, Cd; $C$ = Ni, Co), have been successfully grown, and their structural, magnetic,…

Materials Science · Physics 2026-04-24 Ryoya Nakamura , Shinichiro Asai , Yusuke Nambu , Takatsugu Masuda , Kenta Kimura

A comprehensive study of the structural properties of the heavily investigated rare-earth A2Ir2O7 series under extreme conditions is presented. The series is covered by studying iridates with A = Pr, Sm, Dy-Lu. Temperature- and…

We report a detailed study of structural and magnetic properties of the pyrochlore-type (Bi2-xPrx)Ru2O7 series. Eleven compositions with 0 <= x <= 2 were prepared by solid state reaction at 1050 degrees C and found to form a solid solution…

Materials Science · Physics 2008-12-16 Siwar Zouari , Rafik Ballou , Abdelwaheb Cheikh-Rouhou , Pierre Strobel

The spin glass behavior of Y2Mo2O7 has puzzled physicists for nearly three decades. Free of bulk disorder within the resolution of powder diffraction methods, it is thought that this material is a rare realization of a spin glass resulting…

The floating zone technique is a well-established single crystal growth method in materials research, able to produce volumetrically large specimens with extremely high purities. However, traditional furnace designs have relied on heating…

Materials Science · Physics 2019-04-25 Julian L. Schmehr , Michael Aling , Eli Zoghlin , Stephen D. Wilson

SmCrO$_3$ single crystals were successfully grown utilizing the high-pressure optical floating-zone method and their crystal structure, magnetization behavior, and magnetic phase diagrams were thoroughly investigated. Magnetic studies were…

Strongly Correlated Electrons · Physics 2025-06-05 Ning Yuan , Erik Walendy , Nour Maraytta , Waldemar Hergett , Luca Bischof , Michael Merz , Rüdiger Klingeler

An optically high-quality single crystal of sodium mesitylene sulfonate crystal was successfully grown by a slow evaporation method using methanol as solvent at room temperature. Single-crystal XRD has characterized the material and belongs…