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The least is the best. We introduce a technique to strongly reduce Pt use for photocatalytic hydrogen generation from TiO2 nanotubes. By site-selectively depositing thin layers of Pt only at the mouth of the nanotubes and by a subsequent…

Chemical Physics · Physics 2016-10-18 Nhat Truong Nguyen , Marco Altomare , JeongEun Yoo , Nicola Taccardi , Patrik Schmuki

In the present work we use TiO2 nanotube arrays, carrying a Pt coating that is optimally dewetted, as a photocatalyst to generate H2. In order to achieve a maximum H2-generation efficiency, on the one hand an ideal thermal dewetting of the…

Self-standing TiO$_2$ nanotube layers in the form of membranes are fabricated by self-organizing anodization of Ti metal and a potential shock technique. The membranes were then decorated by sputtering different Pt amounts i) only at the…

Applied Physics · Physics 2020-06-02 Gihoon Cha , Marco Altomare , Nhat Truong Nguyen , Nicola Taccardi , Kiyoung Lee , Patrik Schmuki

We describe a rapid screening technique for determining the optimal characteristics of nano- photocatalysts for the production of H2 on a single surface. Arrays of TiO2 nanotubes (NTs) with a gradient in length and diameter were fabricated…

Materials Science · Physics 2016-10-18 G. Loget , P. Schmuki

In the present work we investigate the photocatalytic hydrogen production (water splitting) activity of different Pt loaded TiO2 nanotube layers. Therefore, we fabricate free standing membranes and fix them in four different configurations:…

Materials Science · Physics 2016-10-14 Gihoon Cha , Kiyoung Lee , JeongEun Yoo , Manuela S. Killian , Patrik Schmuki

In the present work we explore the front- and back-side performance of a photocatalytic platform consisting of self-organized TiO2 nanotube layers formed by complete anodization of Ti metal films evaporated on quartz slides. The adhesion…

Effective co-catalysts are of key importance for photocatalytic H2 generation from aqueous environments. An attractive co-catalyst candidate are AuPt (metastable) alloys due to the synergistic electronic and chemical interaction of the…

Applied Physics · Physics 2020-05-05 Nhat Truong Nguyen , Selda Ozkan , Ondrej Tomanec , Xuemei Zhou , Radek Zboril , Patrik Schmuki

Au nanoparticles at the TiO$_2$ surface can enhance the photocatalytic H$_2$ generation performances owing to their electron transfer co-catalytic ability. Key to maximize the co-catalytic effect is a fine control over Au nanoparticle size…

Applied Physics · Physics 2020-06-05 Seyedsina Hejazi , Marco Altomare , Shiva Mohajernia , Patrik Schmuki

Photocatalytic $H_2$ evolution reactions on pristine TiO$_2$ is characterized by low efficiencies due to trapping and recombination of charge carriers, and due to a sluggish kinetics of electron transfer. Noble metal (mainly Pt, Pd, Au)…

Au and Pt do not form homogeneous bulk alloys as they are thermodynamically not miscible. However, we show that anodic TiO$_2$ nanotubes (NTs) can in-situ be uniformly decorated with homogeneous AuPt alloy nanoparticles (NPs) during their…

Overlaid self-ordering processes: we form anodic self-organized TiO2 nanostumps and exploit them for self-ordering dewetting of Au-Ag sputtered films. This forms ordered particle configurations at tube top (crown position) or bottom (ground…

Materials Science · Physics 2016-10-17 Nhat Truong Nguyen , Marco Altomare , JeongEun Yoo , Patrik Schmuki

We apply high-energy proton ion-implantation to modify TiO2 nanotubes selectively at their tops. In the proton-implanted region we observe the creation of intrinsic co-catalytic centers for photocatalytic H2-evolution. We find proton…

Photocatalytic reactions on TiO2 have recently gained an enormous resurgence because of various new strategies and findings that promise to drastically increase efficiency and specificity of such reactions by modifications of the titania…

Applied Physics · Physics 2020-04-13 Xuemei Zhou , Ning Liu , Patrik Schmuki

Low-dose nitrogen implantation induces in TiO2 nanotubes a co-catalytic activity for photocatalytic H2-evolution. The use of an ion implantation process leads to a N-implanted zone only at the top part of the tubes. The coupling of this top…

In the present work we grow self-organized TiO2 nanotube arrays with a defined and controlled regular spacing between individual nanotubes. These defined intertube gaps allow to build up hierarchical 1D-branched structures, conformally…

Materials Science · Physics 2016-10-27 Nhat Truong Nguyen , Selda Ozkan , Imgon Hwang , Anca Mazare , Patrik Schmuki

The characterization of Pt/TiO2 (Degussa P25) catalyst system using atomic resolution Z-contrast images and electron energy loss spectroscopy in the scanning transmission electron microscope has recently revealed that Pt particles have a…

Materials Science · Physics 2009-11-11 Hakim Iddir , Vladimir Skavysh , Serdar Ogut , Nigel D. Browning

In the present work, extended Argon ion bombardment was used to modify anatase TiO2 nanotube (NTs) layers. In situ X-ray photoelectron spectroscopy revealed a high content of sub-oxide formed (Ti3+, Ti2+ states) in the nanotube layers.…

Materials Science · Physics 2016-10-14 Xuemei Zhou , Ning Liu , Patrik Schmuki

A template-free process for the synthesis of nanocrystalline TiO2 hierarchical microstructures by reactive Pulsed Laser Deposition (PLD) is here presented. By a proper choice of deposition parameters a fine control over the morphology of…

Materials Science · Physics 2013-11-28 F. Di Fonzo , C. S. Casari , V. Russo , M. F. Brunella , A. Li Bassi , C. E. Bottani

We investigate the photocatalytic performance of nanocomposites prepared in a one-step process by liquid-phase exfoliation of graphite in the presence of TiO$_2$ nanoparticles (NPs) at atmospheric pressure and in water, without heating or…

Highly ordered and self supported anatase TiO2 nanoparticle chains were fabricated by calcining conformally TiO2 coated multi-walled carbon nanotubes (MWCNTs). During annealing, the thin tubular TiO2 coating that was deposited onto the…

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