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Scalar couplings of the form J I_1 \cdot I_2 between nuclei impart valuable information about molecular structure to nuclear magnetic-resonance spectra. Here we demonstrate direct detection of J-spectra due to both heteronuclear and…

Atomic Physics · Physics 2015-05-13 M. P. Ledbetter , C. W. Crawford , A. Pines , D. E. Wemmer , S. Knappe , J. Kitching , D. Budker

We present NMR spectra of remote-magnetized deuterated water, detected in an unshielded environment by means of a differential atomic magnetometer. The measurements are performed in a $\mu$T field, while pulsed techniques are applied…

We investigate nuclear magnetic resonance (NMR) in near-zero-field, where the Zeeman interaction can be treated as a perturbation to the electron mediated scalar interaction (J-coupling). This is in stark contrast to the high field case,…

A diamond-based sensor utilizing nitrogen-vacancy (NV) center ensembles permits the analysis of micron-sized samples through NMR techniques at room temperature. Current efforts are directed towards extending the operating range of NV…

Quantum Physics · Physics 2024-10-07 P. Alsina-Bolívar , A. Biteri-Uribarren , C. Munuera-Javaloy , J. Casanova

Ultralow-field nuclear magnetic resonance (NMR) provides a new regime for many applications ranging from materials science to fundamental physics. However, the experimentally observed spectra show asymmetric amplitudes, differing greatly…

Quantum Physics · Physics 2019-02-22 Min Jiang , Wenjie Xu , Yunlan Ji , Ji Bian , Shiming Song , Xinhua Peng

Zero- to ultra-low-field nuclear magnetic resonance (ZULF NMR) provides a new regime for the measurement of nuclear spin-spin interactions free from effects of large magnetic fields, such as truncation of terms that do not commute with the…

We present a method which allows for the extraction of physical quantities directly from zero- to ultralow-field nuclear magnetic resonance (ZULF NMR) data. A numerical density matrix evolution is used to simulate ZULF NMR spectra of…

Chemical Physics · Physics 2018-03-14 Alexander Wilzewski , Samer Afach , John W. Blanchard , Dmitry Budker

Zero- to ultralow-field nuclear magnetic resonance (ZULF NMR) is an alternative spectroscopic method to high-field NMR, in which samples are studied in the absence of a large magnetic field. Unfortunately, there is a large barrier to entry…

Chemical Physics · Physics 2020-04-29 John W. Blanchard , Teng Wu , James Eills , Yinan Hu , Dmitry Budker

An all-optical atomic magnetometer is used to detect a proton free-precession signal from a water sample polarized in a 0.7 T field and remotely analyzed in a 4 $\mu T$ field. Nuclear spins are manipulated either by $\pi/2$ pulses or by…

Atomic Physics · Physics 2015-05-13 Giuseppe Bevilacqua , Valerio Biancalana , Yordanka Dancheva , Luigi Moi

We present single- and multiple-quantum correlation $J$-spectroscopy detected in zero ($<\!\!1$~$\mu$G) magnetic field using a \Rb vapor-cell magnetometer. At zero field the spectrum of ethanol appears as a mixture of \carbon isotopomers,…

Chemical Physics · Physics 2020-08-26 Tobias F. Sjolander , John W. Blanchard , Dmitry Budker , Alexander Pines

An unusual regime for liquid-state nuclear magnetic resonance (NMR) where the magnetic field strength is so low that the $J$-coupling (intramolecular spin-spin) interactions dominate the spin Hamiltonian opens a new paradigm with…

Atomic Physics · Physics 2019-10-02 Dmitry Budker

Zero and ultralow-field nuclear magnetic resonance (ZULF NMR) is an NMR modality where experiments are performed in fields at which spin-spin interactions within molecules and materials are stronger than Zeeman interactions. This typically…

Nuclear magnetic resonance (NMR) schemes can be applied to micron-, and nanometer-sized samples by the aid of quantum sensors such as nitrogen-vacancy (NV) color centers in diamond. These minute devices allow for magnetometry of nuclear…

Quantum Physics · Physics 2021-07-19 C. Munuera-Javaloy , R. Puebla , J. Casanova

We introduce quantum J-oscillators that exploit intrinsic nuclear spin-spin (scalar J) couplings in molecules to produce phase-coherent oscillations. Operated in zero magnetic field and driven by a digital feedback, they operate from…

Quantum Physics · Physics 2026-02-17 Jingyan Xu , Raphael Kircher , Oleg Tretiak , Dmitry Budker , Danila A. Barskiy

We report an optical inelastic-wave-mixing-enhanced atomic magnetometry technique that results in nT-level magnetic field detection at temperatures compatible with the human body without magnetic shielding, zero-field compensation, or…

Quantum Physics · Physics 2018-04-24 Feng Zhou , Eric Y. Zhu , Yvonne L. Li , E. W. Hagley , L. Deng

We present a system developed to premagnetize liquid samples in an ultra-low-field Nuclear Magnetic Resonance (NMR) experiment. Liquid samples of a few milliliter are exposed to a magnetic field of about 70~mT, which is abruptely switched…

Instrumentation and Detectors · Physics 2020-04-22 Valerio Biancalana , Roberto Cecchi , Leonardo Stiaccini , Antonio Vigilante

A multi-channel atomic magnetometer operating in an unshielded environment is described and characterised. The magnetometer is based on D1 optical pumping and D2 polarimetry of Cs vapour contained in gas-buffered cells. Several technical…

Instrumentation and Detectors · Physics 2016-04-14 Giuseppe Bevilacqua , Valerio Biancalana , Piero Chessa , Yordanka Dancheva

We report detection of nuclear magnetic resonance (NMR) using an anisotropic magnetoresistive (AMR) sensor. A ``remote-detection'' arrangement was used, in which protons in flowing water were pre-polarized in the field of a superconducting…

Chemical Physics · Physics 2015-05-13 F. Verpillat , M. P. Ledbetter , D. Budker , S. Xu , D. Michalak , C. Hilty , S. Antonijevic , A. Pines , L. -S. Bouchard

We present a method for the first-principles calculation of nuclear magnetic resonance (NMR) J-coupling in extended systems using state-of-the-art ultrasoft pseudopotentials and including scalar-relativistic effects. The use of ultrasoft…

Materials Science · Physics 2014-08-12 Timothy F. G. Green , Jonathan R. Yates

Nuclear magnetic resonance (NMR) spectroscopy usually requires high magnetic fields to create spectral resolution among different proton species. At low fields, chemical shift dispersion is insufficient to separate the species, and the…

Chemical Physics · Physics 2021-03-03 Stephen J. DeVience , Mason Greer , Soumyajit Mandal , Matthew S. Rosen
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