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Related papers: Stoichiometric YFe2O4-\delta\ single crystals grow…

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We report the controlled growth of single crystals of intercalated layered Lu$ _{1+n} $Fe$ _{2+n} $O$ _{4+3n-\delta} $ ($ n $=1,2) with different oxygen stoichiometries ${\delta}$. For the first time crystals sufficiently stoichiometric to…

Strongly Correlated Electrons · Physics 2019-06-07 Sabreen Hammouda , Manuel Angst

We report the growth of mm-sized Pmnb-Li2FeSiO4 single crystals by means of the optical floating-zone method at high argon pressure and describe the conditions required for a stable growth process. The crystal structure is determined and…

Mm-sized LiMn$_{1-x}$Fe$_x$PO$_4$ single crystals with $0\leq x \leq 1$ were grown by means of the traveling floating-zone technique at elevated Argon pressure of 30~bar. For the various doping levels, the growth process was optimized with…

Strongly Correlated Electrons · Physics 2017-02-07 Christoph Neef , Hubert Wadepohl , Hans-Peter Meyer , Rüdiger Klingeler

The availability of large high-quality single crystals is an important prerequisite for many studies in solid-state research. The optical floating-zone technique is an elegant method to grow such crystals, offering potential to prepare…

CuFeO$_2$ single crystals up to 50 mm in length and up to 10 mm in diameter were grown by the optical floating-zone method. Stoichiometric polycrystalline rods with a diameter of 6-12 mm were used as feed materials to produce crystals of…

Materials Science · Physics 2020-01-07 Nora Wolff , Tobias Schwaigert , Dietmar Siche , Darrell G. Schlom , Detlef Klimm

We report the optimized conditions for growing the high quality single crystals of candidate quantum spin-ice Pr2Hf2O7 using the optical floating-zone method. Large single crystals of Pr2Hf2O7 have been grown under different growth…

Strongly Correlated Electrons · Physics 2019-01-02 V. K. Anand , A. T. M. N. Islam , A. Samartzis , J. Xu , N. Casati , B. Lake

Single crystals of superconducting KxFe2-ySe2 have been grown with the optical floating-zone technique under application of 8 bar of argon pressure. We found that large and high quality single crystals with dimensions of ~\varnothing6…

Superconductivity · Physics 2012-07-09 Y. Liu , Z. C. Li , W. P. Liu , G. Friemel , D. S. Inosov , R. E. Dinnebier , Z. J. Li , C. T. Lin

Single crystal growth of {\alpha}-Na$_x$MnO$_2$ (x = 0.90) is reported via the floating zone technique. The conditions required for stable growth and intergrowth-free crystals are described along with the results of trials under alternate…

MgO single crystals with diameters between 3.5 and 5 mm and lengths up to 40 mm were grown by the optical floating zone technique (OFZ). Despite challenging material properties such as the high melting point of 2825 {\deg}C, very high…

We report on the growth of Y2Ti2O7 single crystals by optical floating zone technique. X-ray diffraction and Raman spectroscopy studies confirm the structural quality of the crystal. The UV-Vis optical studies reveal that the grown crystals…

Materials Science · Physics 2020-06-15 M. Suganya , K. Ganesan , P. Vijayakumar , Amirdha Sher Gill , R. Ramaseshan , S. Ganesamoorthy

We report a study on the crystal growth of the hexagonal manganites $R$MnO$_3$ ($R$ = Y, Lu, Ho, Er, and Tm) by using an optical floating-zone method. It was found that high-quality single crystals of $R$ = Y, Lu, and Ho could be easily…

Strongly Correlated Electrons · Physics 2015-06-17 C. Fan , Z. Y. Zhao , J. D. Song , J. C. Wu , F. B. Zhang , X. F. Sun

The wealth of structural phases seen in the rare-earth disilicate compounds promises an equally rich range of interesting magnetic properties. We report on the crystal growth by the optical floating zone method of members of the rare-earth…

The Fe^{4+}-containing cubic perovskite phase SrFeO_3-x is of interest both for its high-temperature, oxygen-conducting properties as a solid oxide fuel cell component, and at low temperatures, where it exhibits a plethora of helical…

Materials Science · Physics 2012-10-23 D. C. Peets , Jung-hwa Kim , M. Reehuis , P. Dosanjh , B. Keimer

Large single crystals of the pyrochlore Pr2Hf2O7 have been successfully grown by the floating zone technique using an optical furnace equipped with high power Xenon arc lamps. Structural investigations have been carried out by both…

We explore two methods for single crystal growth of the theoretically proposed magnetic Weyl semimetals $R$AlGe ($R$ = Pr,Ce), which prove that a floating zone technique, being both crucible- and flux-free, is crucial to obtain perfectly…

Materials Science · Physics 2019-06-28 P. Puphal , C. Mielke , N. Kumar , Y. Soh , T. Shang , M. Medarde , J. S. White , E. Pomjakushina

We present a route to grow single crystals of Ba$_{0.9}$Sr$_{0.1}$CuSi$_{2}$O$_{6}$ suitable for inelastic neutron studies via the floating zone technique. Neutron single crystal diffraction was utilized to check their bulk quality and…

Materials Science · Physics 2019-07-02 Pascal Puphal , Stephan Allenspach , Christian Rüegg , Ekaterina Pomjakushina

A macroscopic single crystal of $\gamma_{\rm II}$-Li\(_2\)FeSiO\(_4\) has been grown by means of the high-pressure optical floating-zone technique. Static magnetic susceptibility $\chi$ implies that the tetrahedrally-coordinated Fe$^{2+}$…

We report the growth of large single-crystals of Cu2MnAl, a ferromagnetic Heusler compound suitable for polarizing neutron monochromators, by means of optical floating zone under ultra-high vacuum compatible conditions. Unlike Bridgman or…

A series of Yb2Ti2O7 doped samples demonstrates the effects of off-stoichiometry on Yb2Ti2O7's structure, properties, and magnetic ground state via x-ray diffraction, specific heat, and magnetization measurements. A stoichiometric single…

Strongly Correlated Electrons · Physics 2017-03-15 K. E. Arpino , B. A. Trump , A. O. Scheie , T. M. McQueen , S. M. Koohpayeh

High-quality single crystals are essentially needed for the investigation of the novel bulk properties of unconventional superconductors. The availability of such crystals grown by the floating-zone method has helped to unveil the…

Superconductivity · Physics 2019-01-08 J. S. Bobowski , N. Kikugawa , T. Miyoshi , H. Suwa , S. Yonezawa , D. A. Sokolov , A. P. Mackenzie , Y. Maeno
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