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The high-pressure melting curves of metals provide simple and useful tests for theories of melting, as well as important constraints for the modeling of planetary interiors. Here, we present an experimental technique that reveals the latent…

The high pressure and high temperature phase diagram of Ta has been studied in a laser-heated diamond-anvil cell (DAC) using x-ray diffraction measurements up to 52 GPa and 3800 K. The melting was observed at nine different pressures, being…

Materials Science · Physics 2009-11-10 D. Errandonea , M. Somayazulu , D. Hausermann , H. K. Mao

A simple method for detection of melting event in laser-heated diamond anvil cells (DACs) is introduced. The melting is registered optically by the formation of spherical drops of the investigated material as heated in an inert pressure…

Melting experiments require rapid data acquisition due to instabilities of the molten sample and optical drifting due to the high required laser power. In this work, the melting curve of zirconium has been determined for the first time up…

Materials Science · Physics 2019-08-14 Paraskevas Parisiades , Federico Cova , Gaston Garbarino

It is claimed that all of the pressure scales of the reported melting curves derived by diamond anvil cell experiments require a correction which takes into account the pressure thermal shift, where vanadium is an illustrative example. The…

Materials Science · Physics 2022-09-21 Joseph Gal , Lonia Friedlander

Numerical simulations of heat transport in diamond anvil cells reveal a possibility for absolute measurements of specific heat via high-frequency modulation calorimetry. Such experiments could reveal and help characterize temperature-driven…

Materials Science · Physics 2017-04-26 Zachary M. Geballe , Gilbert W. Collins , Raymond Jeanloz

We describe an experimental platform that generates infrared images of micrometer-sized samples in the high pressure region of a diamond anvil cell. Using a 2.3 micron laser as a source of radiation, the system will be particularly useful…

Superconductivity · Physics 2021-11-24 Tarun Patel , A. Drozdov , V. S. Minkov , M. I. Eremets , E. J. Nicol , J. P. Carbotte , T. Timusk , A. W. Tsen

When diamond anvil cell (DAC) sample chambers are outfitted with both thermal insulation and electrodes, two cutting-edge experimental methods are enabled: Joule heating with spectroradiometric temperature measurement, and electrical…

The creation and exploration of new materials under extreme pressure-temperature conditions has become increasingly reliant on laser-heated diamond anvil cell (LHDAC) techniques, which provide direct access to previously unexplored regions…

Materials Science · Physics 2026-05-18 S. Huyan , R. F. S. Penacchio , D. Zhang , Z. Li , S. L. Morelhão , Raquel Ribeiro , P. C. Canfield , S. L. Bud'ko

Tuning the energy density of matter at high pressures gives rise to exotic and often unprecedented properties, e.g., structural transitions, insulator-metal transitions, valence fluctuations, topological order, and the emergence of…

Superconductivity · Physics 2022-09-21 Nathan Dasenbrock-Gammon , Raymond McBride , Gyeongjae Yoo , Sachith Dissanayake , Ranga Dias

Part I shows that quantitative measurements of heat capacity are theoretically possible inside diamond anvil cells via high-frequency Joule heating (100 kHz to 10 MHz), opening up the possibility of new methods to detect and characterize…

Materials Science · Physics 2017-04-26 Zachary M. Geballe , Viktor V. Struzhkin , Andrew Townley , Raymond Jeanloz

The prediction of the melting curve of metals by extrapolation to high pressures and temperatures based on the Lindemann-Gilvarry criterion (LG) assuming harmonic Debye solid is presented. The LG formulation uses the bulk modulus B and its…

Materials Science · Physics 2019-12-16 Joseph Gal

The melting curve and fluid equation of state of carbon dioxide have been determined under high pressure in a resistively-heated diamond anvil cell. The melting line was determined from room temperature up to $11.1\pm0.1$ GPa and $800\pm5$…

Other Condensed Matter · Physics 2016-08-16 Valentina M. Giordano , Frédéric Datchi , Agnès Dewaele

We report a combined experimental and theoretical study of the melting curve and the structural behavior of vanadium under extreme pressure and temperature. We performed powder x-ray diffraction experiments up to 120 GPa and 4000 K,…

Materials Science · Physics 2019-10-02 D. Errandonea , S. G. MacLeod , L. Burakovsky , D. Santamaria-Perez , J. E. Proctor , H. Cynn , M. Mezouar

Accurate and precise measurements of spectroradiometric temperature are crucial for many high pressure experiments that use diamond anvil cells or shock waves. In experiments with sub-millisecond timescales, specialized detectors such as…

Instrumentation and Detectors · Physics 2023-10-26 Zachary M. Geballe , Francesca Miozzi , Chris F. Anto , Javier Rojas , Jing Yang , Michael J. Walter

We performed ac-susceptibility measurements of magnesium diboride powder samples under pure hydrostatic pressures up to 0.4 GPa and under quasi-hydrostatic pressure conditions up to 8 GPa in a helium gas pressure cell and a diamond-anvil…

Superconductivity · Physics 2007-05-23 S. I. Schlachter , W. H. Fietz , K. Grube , W. Goldacker

In situ studies under severe plastic deformation at high pressures, employing rotational/shear diamond anvil cells (RDAC), have recently gained much interest in the high-pressure community owing to their potential applications in material…

Materials Science · Physics 2023-12-22 K. K. Pandey , H. K. Poswal

Pressure is a unique tool to tune the interplay between structural, electronic and magnetic interactions. It leads to remarkable properties of materials such as recent temperature records in superconductivity. Advanced magnetic measurements…

Temperature and pressure are essential parameters in the synthesis, evaluation, and application of functional materials. This study proposes the addition of a heating function to a high-pressure diamond anvil cell (DAC) with in-situ…

Diamond quantum sensors offer high precision and spatial resolution as magnetic probes, making them promising for a wide range of applications. While diamond anvil cells (DACs) can generate extremely high pressures, techniques for…

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