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In the quest of understanding significant variations in the physical, chemical and electronic properties of the novel functional materials, low temperature Synchrotron X-ray Diffraction (LT-SXRD) measurements on CTO (a type-II) and CMTO (a…

Materials Science · Physics 2016-08-09 Harishchandra Singh , A. K. Sinha , M. N. Singh , A. Upadhyay , Archna Sagdeo

We report measurements of structural phase transition of four parent compounds $R$FeAsO ($R$ = La, Sm, Gd, and Tb) by means of low-temperature X-ray diffraction (XRD). Magnetic transition temperatures associated with Fe ions ($T_{N1}$) are…

The low-temperature and high-magnetic field (2K, 8T) powder x-ray diffraction (LTHM-XRD) measurements have been carried out at different temperatures (T) and magnetic fields (H) to investigate the structural phase diagram for phase…

Materials Science · Physics 2015-08-21 Shivani Sharma , Aga Shahee , Kiran Singh , N. P. Lalla , P. Chaddah

Using x-ray powder diffraction technique at various temperatures and applied magnetic fields, we have studied the magnetostructural properties of Ce(Fe0.95Si0.05)2. The x-ray diffraction data establish quantitative relationships between…

Strongly Correlated Electrons · Physics 2010-05-21 Arabinda Haldar , Niraj K. Singh , Ya. Mudryk , K. G. Suresh , A. K. Nigam , V. K. Pecharsky

Neutron powder diffraction studies of the crystal and magnetic structures of the magnetocaloric compound Mn1.1Fe0.9(P0.8Ge0.2) have been carried out as a function of temperature, applied magnetic field, and pressure. The data reveal that…

Materials Science · Physics 2009-11-30 D. M. Liu , Q. Huang , M. Yue , J. W. Lynn , L. J. Liu , Y. Chen , Z. H. Wu , J. X. Zhang

Representative compounds of the new family of magnetic materials Gd5-xNdxSi4 were analyzed by X-ray diffraction at the XRD1 beamline at LNLS. To reduce X-ray absorption, thin layers of the powder samples were mounted outside the capillaries…

Instrumentation and Detectors · Physics 2017-04-21 A. M. G. Carvalho , R. S. Nunes , A. A. Coelho

Case studies of $1T$-TiSe$_2$ and YBa$_2$Cu$_3$O$_{7-\delta}$ have demonstrated that x-ray diffraction (XRD) studies can be used to trace even subtle structural phase transitions which are inherently connected with the onset of…

The design, calibration, and initial application of a non-contact high-temperature furnace developed for in situ synchrotron X-ray experiments are presented. The system enables a stable operation up to 1000 {\deg}C, with heating rates…

Instrumentation and Detectors · Physics 2025-07-02 Louis Lesage , Yves Watier , Helena Isern , Aditya Shukla , Virginia Sanna , Thomas Dufrane , Yubin Zhang , Carsten Detlefs , Can Yildirim

Multiferroic TbMnO3 is investigated using x-ray diffraction in high magnetic fields. Measurements on first and second harmonic structural reflections due to modulations induced by the Mn and Tb magnetic order are presented as function of…

Strongly Correlated Electrons · Physics 2008-07-29 J. Strempfer , B. Bohnenbuck , I. Zegkinoglou , N. Aliouane , S. Landsgesell , M. v. Zimmermann , D. N. Argyriou

Two-dimensional (2D) materials can host stable, long-range magnetic phases in the presence of underlying magnetic anisotropy. The ability to realize the full potential of 2D magnets necessitates systematic investigation of the role of…

A magneto-structural phase transition is investigated in single crystal CrN thin films grown by rf plasma molecular beam epitaxy on MgO(001) substrates. While still within the vacuum environment following MBE growth, $\it in-situ$…

X-ray magnetic circular dichroism (XMCD) has become an important and powerful tool because it allows the study of material properties in combination with elemental specificity, chemical state specificity, and magnetic specificity. A new…

Instrumentation and Detectors · Physics 2015-06-19 Zhi-Ying Guo , Cai-Hao Hong , Hai-Ying Xing , Kun Tang , Wei Xui , Dong-liang Chen , Ming-Qi Cui , YI-Dong Zhao

A Mythen detector has been equipped at the beamline 4B9A of Beijing Synchrotron Radiation Facility, which can be used for in-situ real-time measurement of X-ray diffraction (XRD) full profiles. In this paper, the thermal expansion behavior…

Materials Science · Physics 2015-08-19 Rong Du , Zhongjun Chen , Quan Cai , Jianlong Fu , Yu Gong , Zhonghua Wu

We report on the discovery of a large, room temperature magnetoresistance (MR) effect in polyfluorene sandwich devices in weak magnetic fields. We characterize this effect and discuss its dependence on voltage, temperature, film thickness,…

Materials Science · Physics 2016-08-16 T. L. Francis , Ö. Mermer , G. Veeraraghavan , M. Wohlgenannt

Single shot x-ray diffraction (XRD) experiments have been performed with a x-ray free electron laser (XFEL) under pulsed high magnetic fields up to 16 T generated with a nondestructive minicoil. The antiferromagnetic insulator phase in a…

Here we show that the low temperature phase of magnetite is associated with an effective, although fractional, ordering of the charge. Evidence and a quantitative evaluation of the atomic charges are achieved by using resonant x-ray…

Strongly Correlated Electrons · Physics 2009-11-11 E. Nazarenko , J. E. Lorenzo , Y. Joly , J. L. Hodeau , D. Mannix , C. Marin

Perovskite-type manganites, which are well-known for their intriguing physical properties such as colossal magnetoresistance (CMR) and half metalicity, have been considered as candidate materials for spintronics. However, their…

The low temperature lattice structure and magnetic properties of Co$_{2.75}$Fe$_{0.25}$O$_4$ ferrite have been investigated using experimental results from synchrotron x-ray diffraction (SXRD), dc magnetization, ac susceptibility, neutron…

Strongly Correlated Electrons · Physics 2020-07-09 R. N. Bhowmik , Amit Kumar , A. K. Sinha , S. M. Yusuf

Dark field X-ray microscopy (DFXM) is an experimental technique employed to investigate material properties by probing their 'mesoscale,' or microscale structures, in a bulk-sensitive manner using hard X-rays at synchrotron radiation…

Materials Science · Physics 2024-08-19 Jayden Plumb , Ishwor Poudyal , Rebecca L. Dally , Samantha Daly , Stephen D. Wilson , Zahir Islam

The effect of improved dielectric properties in the presence of an applied magnetic field is discussed in Pr doped polycrystalline Gd$_{0.55}$Pr$_{0.45}$MnO$_3$ complemented by the structural properties down to 50 K and magnetic properties.…

Strongly Correlated Electrons · Physics 2023-04-05 Pooja Pant , Harshit Agarwal , Suresh Bharadwaj , Archana Sagdeo , M. A. Shaz
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