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Germanates are often used as structural analogs of planetary silicates. We have explored the high-pressure phase relations in Mg$_2$GeO$_4$ using diamond anvil cell experiments combined with synchrotron x-ray diffraction and computations…

Geophysics · Physics 2024-03-06 R. V. Divya , G. Kumar , R. E. Cohen , S. J. Tracy , Y. Meng , S. Chariton , V. B. Prakapenka , R. Dutta

The effect of Mg-substitution on the crystal structure of wurtzite ZnO is presented based on synchrotron X-ray diffraction studies of polycrystalline Zn1-xMgxO (0 <= x <= 0.15). Increase in Mg concentration results in pronounced c-axis…

Materials Science · Physics 2007-05-23 Young-Il Kim , Katharine Page , Ram Seshadri

The structural evolution of two selected compositions of Yttria-Stabilized Zirconia (YSZ), with 3mol% (3YSZ) and 8mol% (8YSZ) of Y2O3, have been investigated under pressure using in-situ synchrotron X-ray diffraction (XRD) and Raman…

The multiferroic manganese tungstate (MnWO4) has been studied by high-pressure Raman spectroscopy at room temperature under quasi-hydrostatic conditions up to 39.3 GPa. The low-pressure wolframite phase undergoes a phase transition at 25.7…

Materials Science · Physics 2014-01-28 J. Ruiz-Fuertes , D. Errandonea , O. Gomis , A. Friedrich , F. J. Manjon

Raman spectroscopy is a widely used experimental technique to study the vibrational properties of solids. Atomic scale simulations can be used to predict such spectra, but trustworthy studies at finite temperatures are challenging, mainly…

Materials Science · Physics 2025-09-03 Petter Rosander , Erik Fransson , Nicklas Österbacka , Paul Erhart , Göran Wahnström

Vanadium sesquioxide, V2O3, is a prototypical metal-to-insulator system where, in temperature-dependent studies, the transition always coincides with a corundum-to-monoclinic structural transition. As a function of pressure, V2O3 follows…

We did extensive research for the typical nanolaminate Mn+1AXn (n=1, 2, 3) ceramics focusing on the structural stability, the phase transition pressure of Ti2GaN (160 GPa) is far higher than that of Zr2GaN (92 GPa), meaning the strong M…

Materials Science · Physics 2020-12-23 Ben-Yang Li , Fang Chen , Heng-Na Xiong , Ling Tang , Ju-Xiang Shao , Ze-Jin Yang

We report the results of Raman spectroscopy high-pressure studies of alkali metal fluoroargentates (M2AgF4, where M=Na, K, Rb) associated with theoretical and x-ray diffraction studies for the K member of the series. Theoretical density…

High-temperature and high-pressure experiments were conducted on columbite-type ZnNb2O6, reaching temperatures up to 873 K at ambient pressure and pressures up to 30 GPa at ambient temperature, respectively. Through systematic analysis…

Structural, magnetic and electric properties of a metal-ordered perovskite YBaMn2O6 have been studied by means of powder X-ray diffraction, DSC, magnetic susceptibility, and electric resistivity. It is found that this material undergoes a…

Strongly Correlated Electrons · Physics 2009-11-07 T. Nakajima , H. Kageyama , Y. Ueda

We use Raman spectroscopy in tandem with transmission electron microscopy and DFT simulations to show that extreme (GPa) pressure converts the phase of silicon nanowires from cubic (Si-I) to hexagonal (Si-IV) while preserving the nanowire's…

Materials Science · Physics 2016-11-06 Bennett E. Smith , Xuezhe Zhou , Paden B. Roder , Evan H. Abramson , Peter J. Pauzauskie

We investigate the crystal structure and lattice vibrations of Sr$_2$IrO$_4$ by a combined phonon Raman scattering and x-ray powder diffraction experiment under pressures up to $66$ GPa and room temperature. Density functional theory (DFT)…

Strongly Correlated Electrons · Physics 2018-09-05 K. Samanta , F. M. Ardito , N. M. Souza-Neto , E. Granado

The luminescence and Raman spectra of the Cs2ZrCl6 crystal in a wide range of pressures were studied in this work for the first time. Luminescence measurements were performed up to 10 GPa, while the Raman spectra were measured up to 20 GPa.…

Materials Science · Physics 2024-12-31 L. -I. Bulyk , D. Wlodarczyk , S. S. Nagorny , V. V. Nahorna , P. Wang , A. Suchocki

We study the effect of hydrostatic pressure on the magnetotransport properties of the zirconium pentatelluride. The magnitude of resistivity anomaly gets enhanced with increasing pressure, but the transition temperature $T^{\ast}$ is almost…

Materials Science · Physics 2017-05-24 J. L. Zhang , C. Y. Guo , X. D. Zhu , L. Ma , G. L. Zheng , Y. Q. Wang , L. Pi , Y. Chen , H. Q. Yuan , M. L. Tian

Mg2GeO4 is an analogue for the ultra-high pressure behavior of Mg2SiO4, so we have investigated magnesium germanate to 275 GPa and over 2000 K using a laser-heated diamond anvil cell combined with in situ synchrotron X-ray diffraction and…

We investigate the structural, vibrational, morphological, and electronic properties of Nb substituted orthovanadate LaV$_{1-x}$Nb$_x$O$_4$ samples prepared by the solid-state reaction method. The x-ray diffraction (XRD) analysis reveals…

Materials Science · Physics 2023-07-04 Ashok Kumar , Anurag Sharma , Madhav Sharma , Vinod Singh , Anita Dhaka , Rajendra S. Dhaka

Temperature-dependent synchrotron powder diffraction on Cs0.83(Fe0.86Se)2 revealed first order I4/m to I4/mmm structural transformation around 216{\deg}C associated with the disorder of the Fe vacancies. Irreversibility observed during the…

Materials Science · Physics 2011-11-01 V. Svitlyk , D. Chernyshov , E. Pomjakushina , A. Krzton-Maziopa , K. Conder , V. Pomjakushin , V. Dmitriev

The high pressure phase diagram of CsC8 graphite intercalated compound has been investigated at ambient temperature up to 32 GPa. Combining X-ray and neutron diffraction, Raman and X- ray absorption spectroscopies, we report for the first…

Results of in situ high pressure x-ray powder diffraction on the mixed valence compound Cs2Au(I)Au(III)I6 (CsAuI3) are reported, for pressures up to 21 GPa in a diamond anvil cell under hydrostatic conditions. We find a reversible…

Strongly Correlated Electrons · Physics 2013-02-07 Shibing Wang , Shigeto Hirai , Maxwell C. Shapiro , Scott C. Riggs , Theodore H. Geballe , Wendy L. Mao , Ian R. Fisher

High-pressure synchrotron based angle dispersive x-ray diffraction (ADXRD) studies were carried out on SmGdO3 (SGO) up to 25.7GPa at room temperature. ADXRD results indicated a reversible pressure-induced phase transition from ambient…

Materials Science · Physics 2015-06-22 Yogesh Sharma , Pankaj Misra , Satyaprakash Sahoo , A. K. Mishra , S. M. Sharma , Ram S. Katiyar
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