Related papers: One-step method to grow Ba0.6K0.4Fe2As2 single cry…
We present heat capacity, c-axis thermal expansion and pressure dependent, low field, temperature dependent magnetization for pressures up to ~ 12 kbar, data for KFe2As2 single crystals. Tc decreases under pressure with dTc/dP ~ -0.10…
La$_{0.4}$Na$_{0.6}$Fe$_2$As$_2$ single crystals have been grown out of an NaAs flux in an alumina crucible and characterized by measuring magnetic susceptibility, electrical resistivity, specific heat, as well as single crystal x-ray and…
Iron selenide (FeSex) crystals with lateral dimensions up to millimeters were grown via a vapor self-transport method. The crystals consist of the dominant alpha - phase with trace amounts of beta- phase as identified by powder x-ray…
The evolution of pressure induced superconductivity in single crystal as well as polycrystalline samples of BaFe2As2 has been investigated through temperature dependent electrical resistivity studies in 0-7 GPa pressure range. While the…
Magnesium diboride crystals were grown with low melting alloy flux. The sample with superconductivity at 38.3 K was prepared in the zinc-magnesium flux and another sample with superconductivity at 34.11 K was prepared in the…
We report the synthesis and basic physical properties of single crystals of CaFe2As2, an isostructural compound to BaFe2As2 which has been recently doped to produce superconductivity. CaFe2As2 crystalizes in the ThCr2Si2 structure with…
By using high pressure and high temperature (3.7 GPa, 1120 $^{\circ}$C) synthesis technique, we have grown (Cu,C)Ba$_2$Ca$_3$Cu$_4$O$_{11+\delta}$ single crystals. X-ray diffraction, scanning electron microscopy, resistivity and…
We report the successful synthesis of single-crystalline cuprate superconductors HgBa$_{2}$CaCu$_{2}$O$_{6+\delta}$ and HgBa$_{2}$Ca$_{2}$Cu$_{3}$O$_{8+\delta}$. These compounds are well-known for their high optimal superconducting critical…
We report pressure-induced superconductivity in a single crystal of CaFe2As2. At atmospheric pressure, this material is antiferromagnetic below 170 K but under an applied pressure of 0.69 GPa becomes superconducting, with a transition…
The layered honeycomb magnet $\alpha$-RuCl$_3$ is the most promising candidate for a Kitaev quantum spin liquid (KQSL) that can host charge-neutral Majorana fermions. Recent studies have shown significant sample dependence of thermal…
Platelet-like single crystals of the Ca(Fe1-xCox)2As2 series having lateral dimensions up to 15 mm and thickness up to 0.5 mm were obtained from the high temperature solution growth technique using Sn flux. Upon Co doping, the c-axis of the…
A new method for preparation of single crystals of the superconducting intermetallic MgB2 compound from a Mg-Cu-B melt flux is presented. The high vapour pressure of Mg at elevated temperature is a serious challenge of the preparation…
We report on the synthesis of large single crystals of a new FeSe-layer superconductor Cs0.8(FeSe0.98)2. X-ray powder diffraction, neutron powder-diffraction and magnetization measurements have been used to compare the crystal structure and…
In this article we review our studies of the K0.80Fe1.76Se2 superconductor, with an attempt to elucidate the crystal growth details and basic physical properties over a wide range of temperatures and applied magnetic field, including…
Mechanical alloying method has been employed to prepare the Ba-Fe-As-P precursors, necessary for the Ba-(As,P) flux growth of the single crystalline BaFe$_2$(As$_{1-x}$P$_x$)$_2$. By alloying constituent elementals mechanically, the…
(NaxKy)FezSe2 crystals are prepared by Na, Fe, and Se as starting materials in NaCl/KCl flux at low temperatures~720 {\deg}C. It is found that K is more preferred than Na to enter in between FeSe layers and forms the phase. Thus-obtained…
We report on the efficient method of obtaining CeRh$_2$As$_2$ single crystals with the use of a bismuth flux growth method in a horizontal configuration. The crystals thus obtained exhibit much sharper phase transitions and distinctly…
Sizable single crystals of $BaFe_2As_2$ have been grown with self-flux method. The crystals are plate-like with c-axis perpendicular to the plane. The size can be as large as 3 x 5 x 0.2 $mm^3$. The resistivity anisotropy…
Single crystals of MgB2 with a size up to 1.5x0.9x0.2 mm3 have been grown with a high pressure cubic anvil technique. The crystal growth process is very peculiar and involves an intermediate nitride, namely MgNB9. Single crystals of BN and…
Single crystal of La(O,F)BiSe2 was successfully grown for the first time by the CsCl flux method. Single crystal X-ray structural analysis clearly showed that La(O,F)BiSe2 crystalizes with space group P4/nmm (lattice parameters a =…