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Fe2O3 nanoparticles of different sizes ranging from 22 to 56nm were synthesized chemically by a modified sol-gel method. Pure alpha phase particles as well as particles with admixture of alpha and gamma phase were obtained and identified by…

Materials Science · Physics 2007-05-23 Shakeel Akbar , S. K. Hasanain , Nasia Azmat , M. Nadeem

The atomic structure and properties of nanoparticulate Fe2O3 are characterized starting from its smallest Fe2O3 building unit through (Fe2O3)n clusters to nanometer-sized Fe2O3 particles. This is achieved by combining global structure…

Materials Science · Physics 2024-05-30 Andreas Erlebach , Heinz-Dieter Kurland , Janet Grabow , Frank A. Müller , Marek Sierka

Magnetic measurements up to 1000 K have been performed on hydrothermally synthesized $\alpha$-Fe$_{2}$O$_{3}$ nanoparticles (60 nm) using a Quantum Design vibrating sample magnetometer. A high vacuum environment (1$\times$10$^{-5}$ torr)…

Mesoscale and Nanoscale Physics · Physics 2015-05-20 Jun Wang , Wei Wu , Fan Zhao , Guo-meng Zhao

This work reports the successful formation of Ag and Au nanoparticles in $\beta$-Ga$_2$O$_3$ single-crystals by ion implantation and annealing at 550 {\deg}C. X-ray diffraction measurements revealed that nanoparticles were formed after the…

This work gives insights into processing and characterisation of bulk nanocrystalline FeCr materials. The investigated FeCr alloys, consisting of 30, 50 and 70 at.% ferromagnetic Fe and remaining anti-ferromagnetic Cr, are processed by arc…

The six nanosized PrF3 samples were synthesized using two different chemical reactions and different time of hydrothermal reaction. The X-ray and HRTEM experiments showed high crystallinity of synthesized samples. For all samples the…

Thin films of uniformly distributed Fe2O3 nanoparticles have been prepared on single crystal silicon and glass substrates by a spray pyrolysis technique in a single step using a mixture of water and ferrocene dissolved in xylene. The size…

Applied Physics · Physics 2020-05-07 Dayanand , Meenu Chahar , Devesh Kumar Pathak , O. P. Thakur , V. D. Vankar , Rajesh Kumar

Nanolaminated Al2O3/HfO2 thin films as well as single Al2O3 and HfO2 layers have been grown as gate dielectrics by Plasma Enhanced Atomic Layer Deposition (PEALD) technique on silicon carbide (4H-SiC) substrates. All the three dielectric…

Applied Physics · Physics 2021-04-29 Raffaella Lo Nigro , Emanuela Schilirò , Patrick Fiorenza , Fabrizio Roccaforte

At the nanometric scale, the synthesis of a random alloy (i.e. without phase segregation, whatever the composition) by chemical synthesis remains a not easy task, even for simple binary type systems. In this context, a unique approach based…

Due to its multiferroic properties and narrow optical bandgap, Bismuth ferrite has been widely explored for spintronics, photovoltaics, and photocatalysis applications. Bismuth ferrite can be synthesized in various forms like bulk, thin…

Materials Science · Physics 2025-09-10 Naresh Prajapati , G. Surya Prakash , Manoj Kumar , Himanshu Pandey

BiFe1-xCrxO3 (x=0.0, 0.05 and 0.1) nanoparticles are prepared by a combustion method without using any solvent. All the synthesized nanoparticles are single phase in nature, nearly spherical in shape and crystallize in distorted perovskite…

Materials Science · Physics 2015-02-23 Samar Layek , Santanu Saha , H. C. Verma

Iron oxide nano particles with nominal Fe2O3 stoichiometry were synthesized by a wet, soft chemical method with the heat treatment temperatures from 250{\deg}C to 900{\deg}C in air. The variation in the structural properties of the nano…

Materials Science · Physics 2011-11-29 Debajeet K. Bora , Artur Braun , Selma Erat , Olga Safonova , Thomas Graule , Edwin C. Constable

The nucleation and structure of silicon nanocrystals formed by different preparation conditions and silicon concentration (28 - 70 area %) have been studied using Transmission Electron Microscopy (TEM), Energy Filtered TEM (EFTEM) and…

Photoelectrochemical (PEC) water splitting is a promising method for conversing solar energy into chemical energy stored in the form of hydrogen. Nanostructured hematite ($\alpha$-Fe$_2$O$_3$) is one of the most attractive materials for…

Atomic structure of a mono-dispersive hematite ($\alpha$-Fe$_2$O$_3$) nanocube $(0 1\bar1 2)$ surface was determined with synchrotron X-ray diffraction. The $\alpha$-Fe$_2$O$_3$ nanocubes were prepared through a hydrothermal process and a…

Mesoscale and Nanoscale Physics · Physics 2020-06-09 Chang-Yong Kim

This work reports the formation of nano- crystalline Al50Cu28Fe22 by high-energy milling. For obtaining the nano-crystalline material, the Al50Cu28Fe22 alloy synthesized through slow cooling of the molten alloy was subjected to ball…

Materials Science · Physics 2007-05-23 T. P. Yadav , N. K. Mukhopadhyay , R. S. Tiwari , O. N. Srivastava

The experiment was conducted to synthesize carbon nanospheres of different sizes by controlling the temperature in polycondensation reaction of glucose under hydrothermal process. The surface morphology, structural, optical, and thermal…

Materials Science · Physics 2017-06-20 Priya Karna , Sunil Karna

The present study investigates the effect of different reaction times on the crystallinity, surface morphology and size of iron oxide nanoparticles. In this synthetic system, aqueous iron (III) nitrate (Fe(NO$_3$)$_3\cdot9$H$_2$O)…

Applied Physics · Physics 2021-10-29 Ioannis Papagiannis , Mauro S. Innocente , Evangelos I. Gkanas

A method of preparing the nanoparticles of CaCu3Ti4O12 (CCTO) with the crystallite size varying from 30 to 200 nm is optimized at a temperature as low as 680 1C from the exothermic thermal decomposition of an oxalate precursor,…

Materials Science · Physics 2013-01-18 P. Thomas , K. Dwarakanath , K. B. R. Varma , T. R. N. Kutty

Single phase BiFeO3 nanoparticles have been successfully synthesized for the first time by a novel citrate combustion method without using any solvent. Well mixed metal nitrates along with citric acid which is used as fuel combust to give…

Materials Science · Physics 2015-02-23 Samar Layek , H. C. Verma
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