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Structural, vibrational and dielectric properties of (Pb1-xBix)(Ti1-xMnx)O3 (PBTM) (0 x 0.50) polycrystalline ceramics have been examined as a function of temperature. Synchrotron-based powder x-ray diffraction was employed to confirm phase…

We investigated the crystal and magnetic structures of the spin-1/2 frustrated antiferromagnet Cu3Mo2O9 in which the spin system consists of antiferromagnetic chains and dimers. The space group at room temperature has been reported to be…

Through powder x-ray diffraction we have investigated the structural behavior of SmVO3, in which orbital and magnetic degrees of freedom are believed to be closely coupled to the crystal lattice. We have found, contrary to previous reports,…

New fluoropnictides BaMnPnF with Pn = As, Sb, Bi, are synthesized by stoichiometric reaction of elements with BaF\_2. The compounds crystallize in the tetragonal P4/nmm (No. 129, Z = 2) space group, with the ZrCuSiAs-type structure, as…

Strongly Correlated Electrons · Physics 2013-07-09 Bayrammurad Saparov , David J. Singh , V. Ovidiu Garlea , Athena S. Sefat

We applied synchrotron single-crystal X-ray diffraction in a diamond anvil cell at 48-51 GPa and first-principles theoretical calculations to study the crystal structure of solid atomic iodine at high pressure. We report the synthesis of…

We report the synthesis and structural study of mixed oxides in the Ln2ScNbO7 series. New phases with Ln = Pr, Eu, Gd and Dy are obtained. All crystallize in the cubic pyrochlore structure type, space group F-d3m, with no Sc-Nb ordering on…

Materials Science · Physics 2008-12-16 Siwar Zouari , Rafik Ballou , Abdelwaheb Cheikh-Rouhou , Pierre Strobel

We report on the single phase synthesis and room temperature structural characterization of PbFe0.67W0.33O3 (PFW) multiferroic. The PFW was synthesized by low temperature sintering, Columbite method. Analysis of powder XRD pattern exhibits…

Materials Science · Physics 2015-01-07 Shidaling Matteppanavar , Basavaraj Angadi , Sudhindra Rayapro

Millimeter sized single crystals of Mo3Sb7 are grown using the self-flux technique and a thorough characterization of their structural, magnetic, thermal and transport properties is reported. The structure parameters for the…

Superconductivity · Physics 2013-05-24 J. -Q. Yan , M. A. McGuire , A. F. May , H. Cao , A. D. Christianson , D. G. Mandrus , B. C. Sales

We report on the synthesis and on basic superconducting properties of a completely new Mo_2Re_3B ternary boride. The crystal structure of the Mo_2Re_3B compound is characterised by Pmmm space group and the cell parameters: a=11.626 A,…

Superconductivity · Physics 2012-12-24 B. Andrzejewski

Structural and magnetic properties of the geometrically frustrated layered compound YBaCo4O7 have been studied by magnetization and neutron diffraction. A layered type crystal structure, with alternating tetrahedral layers of Kagom\'e and…

Strongly Correlated Electrons · Physics 2015-02-13 A. K. Bera , S. M. Yusuf , S. Banerjee

We report sample preparation, structure, electrical resistivity, magnetic susceptibility and heat capacity studies of a new compound Yb$_2$Ir$_3$Ge$_5$. We find that this compound crystallizes in an orthorhombic structure with a space group…

Strongly Correlated Electrons · Physics 2009-11-10 Yogesh Singh , S. Ramakrishnan

A structural transition at $T\approx 322$ K from the $Pmmm$ to $Pmma$ phase is found to coincide with an anomaly of resistivity. Another structural phase transition doubling the lattice parameter $c$, which has been postulated earlier to…

We have used single crystal X-ray diffraction methods to establish the crystal structures of a compound in the Pd-Mn-Si system and in the Pd-Mn-Ge system. The title compounds have structures related to the Fe$_2$P structure type and are…

Materials Science · Physics 2007-06-16 Srinivasa Thimmaiah , Claudia Felser , Ram Seshadri

We present here the comprehensive X-ray diffraction (XRD) and dielectric measurement of (1-x)Bi(Zn1/2Ti1/2)O3-xPbTiO3 (BZT-xPT) piezoceramics with x=0.65, 0.70, 0.75 and 0.80. Powder X-ray diffraction data reveals the tetragonal structure…

Materials Science · Physics 2013-11-19 Jyoti Sharma , Rishikesh Pandey , Akhilesh Kumar Singh

We report high-resolution neutron powder diffraction on Sr0.61Ba0.39Nb2O6, SBN61, in the temperature range 15-500 K. The results indicate that the low-temperature anomalies (T<100K) observed in the dielectric dispersion are due to small…

Materials Science · Physics 2007-05-23 J. Schefer , D. Schaniel , V. Pomjakushin , U. Stuhr , V. Petricek , Th. Woike , M. Wohlecke , M. Imlau

The domain structure of (1-x)Pb(Mg1/3Nb2/3)O3- xPbTiO3 single crystals with composition x ~ 0.33 in the range of the morphotropic phase boundary (MPB) was studied. Based on the analysis of spontaneous strain compatibility and charge of…

Materials Science · Physics 2009-11-10 A. A. Bokov , Z. -G. Ye

Mn3TeO6 exhibits a corundum-related A3TeO6 structure and a complex magnetic structure involving two magnetic orbits for the Mn atoms [*]. Mn3-xCdxTeO6 (x=0, 1, 1.5 and 2) ceramics were synthesized by solid state reaction and investigated…

Materials Science · Physics 2012-01-20 S. A. Ivanov , R. Mathieu , P. Nordblad , E. Politova , R. Tellgren , C. Ritter , V. Proidakova

Contrary to previous studies that identified the ground state crystal structure of the entire R_3Co series (R is a rare earth) as orthorhombic Pnma, we show that Y_3Co undergoes a structural phase transition at T_t=160K. Single crystal…

Materials Science · Physics 2013-07-18 A. Podlesnyak , G. Ehlers , H. Cao , M. Matsuda , M. Frontzek , O. Zaharko , V. A. Kazantsev , A. F. Gubkin , N. V. Baranov

Single-crystalline CeRh3Si2 was investigated by means of x-ray diffraction, magnetic susceptibility, magnetization, electrical resistivity, and specific heat measurements carried out in wide temperature and magnetic field ranges. Moreover,…

Strongly Correlated Electrons · Physics 2015-05-18 A. P. Pikul , D. Kaczorowski , Z. Gajek , J. Stepien--Damm , A. Slebarski , M. Werwinski , A. Szajek

Results of high resolution x-ray diffraction experiments are presented for single crystals of the spin gap compound BaCuSi$_2$O$_6$ in the temperature range from 16 to 300 K. The data show clear evidence of a transition from the room…

Strongly Correlated Electrons · Physics 2009-11-11 E. C. Samulon , Z. Islam , S. E. Sebastian , P. B. Brooks , M. K. McCourt , J. Ilavsky , I. R. Fisher