Related papers: Crystal growth and superconductivity of FeSe_x
Single crystals FeSex were grown in an evacuated sealed quartz tube using polycrystalline material by gas-transport reaction with I2 as a gas-carrier. Crystals with hexagonal-prismatic, tetragonal-prismatic, planar-square and hexagonal…
A flux-free solution to the growth of large and composition homogeneous superconducting FeSe crystal is reported for the first time, which is based on the traveling-solvent floating-zone technique. The size of the crystal samples prepared…
Single crystals of tetragonal Fe1.00Se were grown from polycrystalline material by chemical vapor transport reaction at temperatures below 723 K using AlCl3 as transport additive. The plate-shaped single crystals have edge lengths up to 4…
We have synthesized single crystals of FeTe1-xSx and investigated the structural and physical properties. The actual S concentration was found to be significantly smaller than the starting nominal value. The solubility limit of S for the Te…
We report flux free growth of superconducting FeSe single crystals by an easy and versatile high temperature melt and slow cooling method for first time. The room temperature XRD on the surface of the piece of such obtained crystals showed…
A new approach to grow FeSe1-xTex single crystals with optical zone-melting technique was successfully employed. Crystals with actual composition 0.4 < x < 1.0 all show high crystallinity with no phase separation. The ability to visually…
Single crystals of superconducting KxFe2-ySe2 have been grown with the optical floating-zone technique under application of 8 bar of argon pressure. We found that large and high quality single crystals with dimensions of ~\varnothing6…
Here, we report self flux single crystal growth of FeTe1-xSex for x = 0 to 0.50 series via solid state reaction route,the resulted crystals as seen are shiny. X Ray diffraction performed on the surface of crystals elucidated the growth in…
Iron selenide (FeSex) crystals with lateral dimensions up to millimeters were grown via a vapor self-transport method. The crystals consist of the dominant alpha - phase with trace amounts of beta- phase as identified by powder x-ray…
We successfully grew the high-quality single crystals of $A_{x}$Fe$_2$Se$_2$ ($A$ = K and Cs) by self-flux method. Sharp superconducting transition was observed for both types of crystals. The crystals show the onset superconducting…
We report self flux growth and characterization of FeTe1-xSx (x= 0.00 to 0.25) single crystal series. Surface X-ray diffraction (XRD) exhibited crystalline nature with growth in (00l) plane. Micro-structural (electron microscopy) images of…
Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…
We report on the synthesis of superconducting single crystals of FeSe, and their characterization by X-ray diffraction, magnetization and resistivity. We have performed ac susceptibility measurements under high pressure in a hydrostatic…
We studied the correlation among structure and transport properties and superconductivity in the different $A_x$Fe$_2$Se$_2$ single crystals ($A$ = K, Rb, and Cs). Two sets of (00$l$) reflections are observed in the X-ray single crystal…
High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…
Single crystals of FeSe_1-x_Te_x_ (0.5=<x=<1) have been grown by the Bridgman method. After annealing them at 400 deg for 100 h in vacuum, single crystals of x=0.5-0.9 have exhibited bulk superconductivity. Anisotropic properties of the…
We investigated the superconducting and transport properties in FeTe$_{1-x}$Se$_{x}$ (0.1 $\leq$ $x$ $\leq$ 0.4) single crystals prepared by O$_2$-annealing. Sharp superconducting transition width observed in magnetization measurement and…
The newly discovered superconductor FeSe1-x (x=0.08, Tconset=13.5 K at ambient pressure rising to 27 K at 1.48 GPa) exhibits a structural phase transition from tetragonal to orthorhombic below 70 K at ambient pressure - the crystal…
Superconducting single crystals of SmFeAsO$_{1-x}$ without fluorine doping were grown at a pressure of 3.3 GPa and a temperature of 1350-1450 $^\circ$C by using the self-flux method. Plate-like single crystals of a few-150 $\mu$m in their…
(La,Ce)OBiS2 single crystals are successfully grown using CsCl flux. The obtained single crystals have a plate-like shape with a size of 0.5-2.0 mm and a well-developed ab-plane. The thickness of the crystals increases with a decrease in…