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Elastic neutron scattering studies of an optimized LaFeAsO single crystal reveal that upon cooling, an onset of the tetragonal (T)-to-orthorhombic (O) structural transition occurs at $T_\texttt{S} \approx 156$ K, and it exhibits a sharp…

Superconductivity · Physics 2015-05-19 H. -F. Li , W. Tian , J. -Q. Yan , J. L. Zarestky , R. W. McCallum , T. A. Lograsso , D. Vaknin

CaFe$_2$As$_2$ has been synthesized and found to form in the tetragonal, ThCr$_2$Si$_2$ structure with lattice parameters $a = 3.912(68) \AA$ and $c = 11.667(45) \AA$. Upon cooling through 170 K, CaFe$_2$As$_2$ undergoes a first order,…

Strongly Correlated Electrons · Physics 2009-11-13 N. Ni , S. Nandi , A. Kreyssig , A. I. Goldman , E. D. Mun , S. L. Bud'ko , P. C. Canfield

TThe parent compounds of iron-arsenide superconductors, $A$Fe$_{2}$As$_{2}$ ($A$=Ca, Sr, Ba), undergo a tetragonal to orthorhombic structural transition at a temperature $T_{\mathrm{TO}}$ in the range 135 to 205K depending on the alkaline…

Strongly Correlated Electrons · Physics 2015-05-18 M. A. Tanatar , E. C. Blomberg , A. Kreyssig , M. G. Kim , N. Ni , A. Thaler , S. L. Bud'ko , P. C. Canfield , A. I. Goldman , I. I. Mazin , R. Prozorov

The crystal structure of the layered iron arsenide Sr3Sc2O5Fe2As2 was determined between 300 and 10 K. The lattice parameters of the tetragonal cell decrease anisotropically according to delta(c)/c : delta(a)/a = 4.2, which results in a…

Superconductivity · Physics 2009-11-08 Marcus Tegel , Inga Schellenberg , Franziska Hummel , Rainer Poettgen , Dirk Johrendt

Superconducting poly- and single-crystalline samples of Sm1-xThxFeAsO with partial substitution of Sm3+ by Th4+ were synthesized and grown under high pressure and their structural, magnetic and transport properties are studied. The…

Superconductivity · Physics 2011-05-25 N. D. Zhigadlo , S. Katrych , S. Weyeneth , R. Puzniak , P. Moll , Z. Bukowski , J. Karpinski , H. Keller , B. Batlogg

The temperature dependent electrical resistivity of single crystalline SrFe2As2 and BaFe2As2 has been measured in a liquid medium, modified Bridgman anvil cell for pressures in excess of 75 kbar. These data allow for the determination of…

Superconductivity · Physics 2015-05-13 E. Colombier , S. L. Bud'ko , N. Ni , P. C. Canfield

We report the temperature dependent x-ray powder diffraction of the FeAs-based superconductors in the range between 300 K and 95 K. In the case of NdOFeAs we have detected the structural phase transition from the tetragonal phase, with…

Superconductivity · Physics 2009-01-12 Alessandro Ricci , Michela Fratini , Antonio Bianconi

The magnetization, crystal structure, and thermal expansion of a nearly stoichiometric Sr$_{1.04(3)}$Er$_{2.09(6)}$O$_{4.00(1)}$ single crystal have been studied by PPMS measurements and in-house and high-resolution synchrotron X-ray powder…

Strongly Correlated Electrons · Physics 2014-10-27 Hai-Feng Li , Andrew Wildes , Binyang Hou , Cong Zhang , Berthold Schmitz , Paul Meuffels , Georg Roth , Thomas Brückel

LiCu_2O_2 single crystals were studied in the temperature range 300-1100 K by means of heating-cooling curves of differential thermal analysis (DTA), thermogravimetry (TG), X-ray powder diffraction and electrical measurements. A reversible…

Materials Science · Physics 2013-09-19 S. A. Ivanov , A. A. Bush , K. E. Kamentsev , E. A. Tishchenko , M. Ottosson , R. Mathieu , P. Nordblad

The crystal structure and electrical resistance of the structurally-layered EuFe2As2 have been studied up to 70 GPa and down to temperature of 10 K, using a synchrotron x-ray source and the designer diamond anvils. The room-temperature…

We report the successful growth of high quality single crystals of LiFeAs with lateral sizes up to 5 x 5 mm2 by the Sn-flux method. Electrical resistivity studies reveal that the superconducting onset temperature is 18.2 K with a transition…

Superconductivity · Physics 2010-10-20 Bumsung Lee , Seunghyun Khim , Jung Soo Kim , G. R. Stewart , Kee Hoon Kim

Structural, magnetic, electrical transport, and heat capacity data are reported for single crystals of TlFe1.6Se2. This compound crystallizes in a tetragonal structure similar to the ThCr2Si2 structure, but with vacancies in the Fe layer.…

We report on the crystal and magnetic structures, magnetic, and transport properties of SrMnSb$_2$ single crystals grown by the self-flux method. Magnetic susceptibility measurements reveal an antiferromagnetic (AFM) transition at $T_{\rm…

The tetragonal-to-orthorhombic structural phase transition (SPT) in LaFeAsO (La-1111) and SmFeAsO (Sm-1111) single crystals measured by high resolution x-ray diffraction is found to be sharp while the RFeAsO (R=La, Nd, Pr, Sm)…

Single crystals of EuPd2Sb2 have been grown from PdSb self-flux. The properties of the single crystals have been investigated by x-ray diffraction, magnetic susceptibility chi, magnetization M, electrical resistivity rho, Hall coefficient…

Superconductivity · Physics 2010-11-17 S. Das , K. McFadden , Yogesh Singh , R. Nath , A. Ellern , D. C. Johnston

Single crystals of Rb{0.8}Fe2Se2 are successfully synthesized with the superconducting transition temperatures T_c{onset}= 31 K and T_c{zero}= 28 K. A clear anomaly of resistivity was observed in the normal state at about 150 K, as found in…

Superconductivity · Physics 2011-05-30 Chun-Hong Li , Bing Shen , Fei Han , Xiyu Zhu , Hai-Hu Wen

X-ray and Neutron diffraction as well as muon spin relaxation and M\"ossbauer experiments performed on SrFe$_2$As$_2$ polycrystalls confirm a sharp first order transition at $T_0 = 205$,K corresponding to an orthorhombic phase distortion…

We report the crystal growth and structural, magnetic, conductivity, and specific heat investigations of Rb(1-x)Fe(2-y)Se2 single crystals with varying stoichiometry prepared by self-flux and Bridgman methods. The system exhibits a strongly…

Superconductivity · Physics 2011-11-01 V. Tsurkan , J. Deisenhofer , A. Günther , H. -A. Krug von Nidda , S. Widmann , A. Loidl

We present magnetic and transport properties of PrRh$_{2}$Si$_{2}$ single crystals which exhibit antiferromagnetic order below T$_{N}$ = 68 K. Well defined anomalies due to magnetic phase transition are observed in magnetic susceptibility,…

Strongly Correlated Electrons · Physics 2009-08-28 V K Anand , Z Hossain , G Behr , G Chen , M Nicklas , C Geibel

We present results from a detailed experimental investigation of LaFeAsO, the parent material in the series of "FeAs" based oxypnictide superconductors. Upon cooling this material undergoes a tetragonal-orthorhombic crystallographic phase…