Related papers: Phase diagram analysis and crystal growth of solid…
CuFeO$_2$ single crystals up to 50 mm in length and up to 10 mm in diameter were grown by the optical floating-zone method. Stoichiometric polycrystalline rods with a diameter of 6-12 mm were used as feed materials to produce crystals of…
We report thermal expansion measurements on Ca(Fe_(1-x)Co_x)_2As_2 single crystals with different thermal treatment, with samples chosen to represent four different ground states observed in this family. For all samples thermal expansion is…
The compound CaV2O4 contains V^{+3} cations with spin S = 1 and has an orthorhombic structure at room temperature containing zigzag chains of V atoms running along the c-axis. We have grown single crystals of CaV2O4 and report…
High-quality and sizable single crystals are crucial for studying the intrinsic properties of unconventional superconductors, which are lacking in the 1111 phase of the Fe-based superconductors. Here we report the successful growth of…
We report the results of a systematic investigation of the phase diagram of the iron-based superconductor, Ba1-xKxFe2As2, from x = 0 to x = 1.0 using high resolution neutron and x-ray diffraction and magnetization measurements. The…
The transport properties, phase diagram, and dopant distribution are investigated in systematically Nd doped CaFe_2As_2 single crystals. Coexistence of two superconducting (SC) phases with different critical transition temperature (T_c) is…
We show that one can employ well-established numerical continuation methods to efficiently calculate the phase diagram for thermodynamic systems. In particular, this involves the determination of lines of phase coexistence related to first…
Single crystals of Na$_{1-\delta}$Fe$_{1-x}$T$_x$As with T = Co, Rh have been grown using a self-flux technique. The crystals were thoroughly characterized by powder X-ray diffraction, magnetic susceptibility and electronic transport with…
We have attempted the crystal growth by the traveling-solvent floating-zone (TSFZ) method of La_{2-x}Ba_xCuO_4 with x~1/8, where the superconductivity is strongly suppressed. Under flowing O_2-gas of a high pressure (4 bars), we have…
We report anisotropic thermal expansion of the parent, AEFe2As2 (AE = Ba, Sr, and Ca), compounds. Above the structural/antiferromagnetic phase transition anisotropy of the thermal expansion coefficients is observed, with the coefficient…
The phase-field crystal model is by now widely used in order to predict crystal nucleation and growth. For colloidal solidification with completely overdamped individual particle motion, we show that the phase-field crystal dynamics can be…
The binary phase diagram of the YAlO3 (YAP) - NdAlO3 (NAP) system was determined by differential thermal analysis (DTA) and X-ray powder diffraction (XRD) measurements. High purity nanocrystalline powders and small single crystals of…
Single crystals of BaFe$_2$As$_2$ and (Ba$_{0.55}$K$_{0.45}$)Fe$_2$As$_2$ have been grown out of excess Sn with 1% or less incorporation of solvent. The crystals are exceptionally micaceous, are easily exfoliated and can have dimensions as…
Centimeter sized platelet single crystals of KFe2As2 were grown using a self-flux method. An encapsulation technique using commercial stainless steel container allowed the stable crystal growth lasting for more than 2 weeks. Ternary K-Fe-As…
The oscillating temperature technique was successfully employed to grow large and composition homogeneous CaFeAsF single crystals due to the reduction of nuclei number by temperature oscillation. The largest as-grown CaFeAsF single crystal…
In this article mixed CuInP$_2$(S$_x$Se$_{1-x}$)$_6$ crystals were investigated by broadband dielectric spectroscopy (20 Hz - 3 GHz). From these results the complete phase diagram has been obtained. In the middle part of the phase diagram…
Single crystals of (Ca1-xLax)10(Pt3As8)(Fe2As2)5 (x = 0 to 0.182) superconductors have been grown and characterized by X-ray, microprobe, transport and thermodynamic measurements. Features in the magnetic susceptibility, specific heat and…
The structural properties of the CaFe2As2 have been investigated by x-ray and neutron powder diffraction techniques as a function of temperature. Unambiguous experimental evidence is shown for coexistence of tetragonal and orthorhombic…
Heat capacity and anisotropic thermal expansion was measured for Ba(Fe_{1-x}Co_x)_2As_2 (x = 0, 0.038, 0.074) single crystals. Thermal expansion is anisotropic and, in tetragonal phase, is significantly higher along the c-axis. Previously…
Superconductivity of Ca1-xLaxFe2As2 single crystals with various doping level were investigated via electromagnetic measurements for out-plane (H//c) and in-plane (H//ab) directions. Obvious double superconducting transitions, which can…