English

To see or not to see: Imaging surfactant coated nano--particles using HIM and SEM

Materials Science 2013-08-19 v3

Abstract

Nano--particles are of great interest in fundamental and applied research. However, their accurate visualization is often difficult and the interpretation of the obtained images can be complicated. We present a comparative scanning electron microscopy and helium ion microscopy study of cetyltrimethylammonium--bromide (CTAB) coated gold nano--rods. Using both methods we show how the gold core as well as the surrounding thin CTAB shell can selectively be visualized. This allows for a quantitative determination of the dimensions of the gold core or the CTAB shell. The obtained CTAB shell thickness of 1.0 nm--1.5 nm is in excellent agreement with earlier results using more demanding and reciprocal space techniques.

Keywords

Cite

@article{arxiv.1304.7167,
  title  = {To see or not to see: Imaging surfactant coated nano--particles using HIM and SEM},
  author = {Gregor Hlawacek and Imtiaz Ahmad and Mark A. Smithers and E. Stefan Kooij},
  journal= {arXiv preprint arXiv:1304.7167},
  year   = {2013}
}

Comments

revised version