English

Surface Sensitive Raman Response of Metal-Supported Monolayer MoS$_2$

Materials Science 2025-04-14 v2

Abstract

The Raman spectrum of monolayer (ML) MoS2_2 is remarkably affected by the interaction with metals. In this work we studied ML-MoS2_2 supported by the Ag(111) and Ag(110) surfaces by using a combined experimental and theoretical approach. The MoS2_2 layer was directly grown on atomically clean Ag(111) and Ag(110) surfaces by pulsed laser deposition, followed by in-situ thermal annealing under ultra-high vacuum conditions. The morphology and structure of the two systems were characterized in-situ by scanning tunneling microscopy, providing atomic-scale information on the relation between the MoS2_2 lattice and the underlying surface. Raman spectroscopy revealed differences between the two MoS2_2-metal interfaces, especially concerning the behavior of the out-of-plane A1A'_1 vibrational mode, which splits into two contributions on Ag(110). The metal-induced effects on MoS2_2 vibrational modes are further evidenced by transferring MoS2_2 onto a more inert substrate (SiO2_2/Si), where the MoS2_2 Raman response displays a more ``freestanding-like'' behavior. The experimental data were interpreted with the support of ab-initio calculations of the vibrational modes, which provided insight into the effect of interface properties, such as strain and out-of-plane distortion. Our results highlight the influence of the interaction with metals on MoS2_2 vibrational properties, and show the high sensitivity of MoS2_2 Raman modes to the surface structure of the supporting metal.

Keywords

Cite

@article{arxiv.2504.00208,
  title  = {Surface Sensitive Raman Response of Metal-Supported Monolayer MoS$_2$},
  author = {Francesco Tumino and Sergio Tosoni and Paolo D'Agosta and Valeria Russo and Carlo Enrico Bottani and Andrea Li Bassi and Carlo Spartaco Casari},
  journal= {arXiv preprint arXiv:2504.00208},
  year   = {2025}
}

Comments

This document is the unedited Author's version of a Submitted Work that was subsequently accepted for publication in The Journal of Physical Chemistry C, copyright \c{opyright} 2025 American Chemical Society after peer review. To access the final edited and published work see https://doi.org/10.1021/acs.jpcc.4c06548